Thermosensitive medical image recording material
An image recording and heat-sensitive technology, applied in temperature recording method, copying/marking method, printing, etc., can solve the problems of high resolution, consumption of precious metals, pollution of the environment, etc., and achieve the effect of high resolution and fast development
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Embodiment 1
[0026] The preparation of embodiment 1 dye precursor microcapsule A
[0027] Put 8g ODB-2, 5ga-methylnaphthalene, and 30g ETAC into the same beaker, stir, and heat in an automatic constant temperature electric heating mantle to dissolve ODB-2 in the high boiling point solvent α-methylnaphthalene and low boiling point solvent In the mixed solvent of ETAC, take it out and cool it to room temperature, ODB-2 cannot be precipitated; put 20ml of D-110 into it, stir to get the oil phase mixture.
[0028] Measure 135ml of PVA-224 aqueous solution with a concentration of 3% and put it into a shear tank, add 20ml of surfactant, and the water phase is ready
[0029] The water phase was sheared at a high speed by a high-speed hardening shear at a speed of 13,000 rpm, and then the oil phase was added to the water phase, emulsified and dispersed for 10 minutes to obtain an oil-in-water emulsion. Add 300 ml of deionized water and 8 grams of tetraethylenepentamine to the oil emulsion dispers...
Embodiment 2
[0030] The preparation of embodiment 2 dye precursor microcapsules B
[0031] Put 8g ODB-2, 5ga-methylnaphthalene, and 30g ETAC into the same beaker, stir, and heat in an automatic constant temperature electric heating mantle to dissolve ODB-2 in the high boiling point solvent α-methylnaphthalene and low boiling point solvent In the mixed solvent of ETAC, take it out and cool it to room temperature, ODB-2 cannot be precipitated; put 20ml of D-110 into it, stir to get the oil phase mixture.
[0032] Measure 135ml of PVA-224 aqueous solution with a concentration of 3% and put it into a shear tank, add 10ml of surfactant, and the water phase is ready
[0033] The water phase was sheared at a high speed by a high-speed solidifying shear at a speed of 7000 rpm, and then the oil phase was added to the water phase, emulsified and dispersed for 10 minutes to obtain an oil-in-water emulsion. In the oil emulsion dispersion, add deionized water 300ml, tetraethylenepentamine 8 grams, the...
Embodiment 3
[0034] The preparation of embodiment 3 dye precursor microcapsules C
[0035] Put 8g ODB-2, 5ga-methylnaphthalene, and 30g ETAC into the same beaker, stir, and heat in an automatic constant temperature electric heating mantle to dissolve ODB-2 in the high boiling point solvent α-methylnaphthalene and low boiling point solvent In the mixed solvent of ETAC, take it out and cool it to room temperature, ODB-2 cannot be precipitated; put 20ml of D-110 into it, stir to get the oil phase mixture.
[0036] Measure 135ml of PVA-224 aqueous solution with a concentration of 3% and put it into a shear tank, add 20ml of surfactant, and the water phase is ready
[0037] The water phase was sheared at a high speed by a high-speed hardening shear at a speed of 14,000 rpm, and then the oil phase was added to the water phase, emulsified and dispersed for 10 minutes to obtain an oil-in-water emulsion. Add 300 ml of deionized water and 8 grams of tetraethylenepentamine to the oil emulsion dispersi...
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