Method for preparing reinforced nickel-based superalloy composite material single crystal blade
A technology of nickel-based superalloy and single crystal blade, which is applied in the field of aerospace materials, can solve the problems of low mechanical properties, short fatigue life at high temperature, etc., and achieve the effects of improving thermal conductivity, strong sintering driving force, and easy diffusion
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Embodiment 1
[0037] 2 micron spherical ultra-fine single crystal nickel powder is used, and 0.3wt% graphene powder is added. The added graphene is a single layer with a carbon content greater than 99% and a specific surface area greater than 80m 2 / g, the conductivity is greater than 1000S / m, and according to the material formula, add spherical ultrafine metal powders less than 5 microns in proportion, such as tungsten, molybdenum, chromium, cobalt, rhenium, ruthenium, aluminum, tantalum, etc., and mix them by ball milling in ethanol solvent Uniform, use the 3D printing process to form the blank of the blade, and then carry out regional melting and alloying on the blank, and at the same time form a large temperature gradient in the melting area for directional solidification, and apply an external electromagnetic field before and after the melting area to force the disordered tiny Orientation of magnetic domains of nickel powder single crystals, confinement induces directional growth of nic...
Embodiment 2
[0039] Apply 2 micron spherical ultrafine polycrystalline nickel powder, add 0.3wt% carbon nanotube powder, the added carbon nanotube is a single-walled carbon nanotube, the diameter is less than 4 μm, the length is less than 30 μm, and the purity is greater than 95%. Surface area greater than 400m 2 / g, the conductivity is greater than 150S / m, and according to the material formula, add spherical ultrafine metal powders such as tungsten, molybdenum, chromium, cobalt, rhenium, ruthenium, aluminum, tantalum, etc. in proportion, and mix them by ball milling in ethanol solvent Uniform, use the powder molding process to form the blank of the blade, and then carry out regional melting and alloying on the blank, and at the same time form a large temperature gradient in the melting area for directional solidification, and apply an external electromagnetic field before and after the melting area to force the disordered The orientation of the magnetic domains of the micro-nickel powder ...
Embodiment 3
[0041] Apply 2 micron spherical ultrafine polycrystalline nickel powder, add 0.3wt% carbon fiber powder, the added carbon fiber is carbon fiber powder with high thermal conductivity, the diameter is less than 50 μm, the length is less than 500 μm, the carbon content is greater than 99%, and the specific surface area is greater than 0.4m 2 / g, the electrical conductivity is greater than 1000S / m, and the thermal conductivity is greater than 400W / mK. At the same time, according to the material formula, tungsten, molybdenum, chromium, cobalt, rhenium, ruthenium, aluminum, tantalum and other spherical ultrafine metal powders are added in proportion , mixed evenly by ball milling in an ethanol solvent, using the powder molding process to form blade blanks, and then carry out regional melting and alloying on the blanks, and at the same time form a large temperature gradient in the melting area for directional solidification, and apply it before and after close to the melting area The...
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