Soaping agent and method for preparing same

A technology of soaping agent and powder, which is applied in the field of soaping agent and its preparation, can solve problems such as unqualified color fastness, and achieve the effect of low raw material price, good economic benefits, safe and simple operation

Inactive Publication Date: 2018-03-09
无锡德冠生物科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

If the temperature is lowered, the color fastness is unqualified

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0043] The invention discloses a soaping agent, which comprises the following components in parts by weight: 20 parts of maleic anhydride-polypropylene copolymer, 5 parts of ammonium persulfate, 5 parts of sodium lignosulfonate, and 5 parts of sodium bicarbonate , 3 parts of polymethylsiloxane, 5 parts of ammonium chloride, 3 parts of chitosan, 3 parts of glyceryl oleate, 5 parts of vegetable powder, 10 parts of ethanol, 3 parts of triethanolamine, 30 parts of deionized water.

[0044] The present invention also provides a kind of preparation method of soaping agent, concrete steps are as follows:

[0045] Step 1, add 30 parts of deionized water, 20 parts of maleic anhydride-polypropylene copolymer, 5 parts of ammonium persulfate, and 3 parts of polymethylsiloxane into the reactor, raise the temperature to 50°C, and protect it under nitrogen. 500 rpm, stirring for 20 minutes;

[0046] Step 2, first disperse 5 parts of plant powder, 10 parts of ethanol, and 3 parts of triethan...

Embodiment 2

[0053]The invention discloses a soaping agent, which comprises the following components in parts by weight: 25 parts of maleic anhydride-polypropylene copolymer, 6 parts of ammonium persulfate, 8 parts of sodium lignosulfonate, and 8 parts of sodium bicarbonate , 4 parts of polymethylsiloxane, 8 parts of ammonium chloride, 4 parts of chitosan, 4 parts of glyceryl oleate, 8 parts of vegetable powder, 15 parts of ethanol, 4 parts of triethanolamine, and 40 parts of deionized water.

[0054] The present invention also provides a kind of preparation method of soaping agent, concrete steps are as follows:

[0055] Step 1, add 40 parts of deionized water, 25 parts of maleic anhydride-polypropylene copolymer, 6 parts of ammonium persulfate, and 4 parts of polymethylsiloxane into the reactor, raise the temperature to 55°C, and protect it under nitrogen. 900 rpm, stirring for 25 minutes;

[0056] Step 2, first disperse 8 parts of plant powder, 15 parts of ethanol, and 4 parts of triet...

Embodiment 3

[0063] The invention discloses a soaping agent, which comprises the following components in parts by weight: 30 parts of maleic anhydride-polypropylene copolymer, 7 parts of ammonium persulfate, 10 parts of sodium lignosulfonate, and 10 parts of sodium bicarbonate , 5 parts of polymethylsiloxane, 10 parts of ammonium chloride, 5 parts of chitosan, 5 parts of glyceryl oleate, 10 parts of plant powder, 20 parts of ethanol, 5 parts of triethanolamine, and 50 parts of deionized water.

[0064] The present invention also provides a kind of preparation method of soaping agent, concrete steps are as follows:

[0065] Step 1, add 50 parts of deionized water, 30 parts of maleic anhydride-polypropylene copolymer, 7 parts of ammonium persulfate, and 5 parts of polymethylsiloxane into the reactor, raise the temperature to 60°C, and protect it under nitrogen. 1000 rpm, stirring for 30 minutes;

[0066] Step 2, first disperse 10 parts of plant powder, 20 parts of ethanol, and 5 parts of tr...

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PUM

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Abstract

The invention discloses a soaping agent and a method for preparing the same. The soaping agent comprises, by weight, 20-30 parts of maleic anhydride-polypropylene copolymers, 5-7 parts of ammonium persulfate, 5-10 parts of sodium lignin sulfonate, 5-10 parts of sodium bicarbonate, 3-5 parts of polymethylhydrosiloxane, 5-10 parts of ammonium chloride, 3-5 parts of chitosan, 3-5 parts of triolein, 5-10 parts of plant powder, 10-20 parts of ethyl alcohol, 3-5 parts of triethanolamine and 30-50 parts of deionized water. The soaping agent and the method have the advantages that the soaping agent isused for removing reactive dye which is not fixed, and the soaping temperatures can be lowered; processes for manufacturing the soaping agent are simple and are easy to implement, raw materials for the soaping agent are low in cost and are easily available, and the soaping agent is non-toxic and harmless and is free of irritation on human bodies and low in volatility.

Description

technical field [0001] The invention belongs to the technical field of textile auxiliaries, and more specifically relates to a soaping agent and a preparation method thereof. Background technique [0002] Soaping mainly refers to the post-printing and dyeing process. After the fiber fabric is printed and dyed, in order to improve its color fastness and brilliance, soap or detergent solution is used to remove unfixed dyes, dyeing auxiliaries, The processing technology of printing paste and so on under the condition of near boiling. [0003] Reactive dyes have complete color spectrum, bright color, low cost and mature dyeing process. Therefore, more than 80% of cellulose fibers are dyed and printed with reactive dyes. There are many kinds of reactive dyes with various chemical structures and different reaction efficiencies, but none of them can fully react with cellulose fibers. In addition, while dyeing and fixing fibers, the dyes will also undergo hydrolysis, that is, the r...

Claims

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Application Information

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Patent Type & AuthorityApplications(China)
IPC IPC(8): C11D1/30C11D3/60C11D3/37C11D3/04C11D3/10C11D3/22C11D3/20C11D3/382C11D3/30
CPCC11D1/30C11D3/046C11D3/10C11D3/201C11D3/2093C11D3/227C11D3/30C11D3/373C11D3/3765C11D3/382
Inventor储平徐有琦
Owner无锡德冠生物科技有限公司