Pharmaceutical preparation and preparation method thereof
A tablet and compound technology, applied in the field of pharmaceutical preparations and its preparation, can solve problems such as channel gating defects, no drugs available, and reduced transport of anions across epithelial cells
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[0401] XRPD (X-ray powder diffraction)
[0402] X-ray diffraction (XRD) data for Compound 1, Compound 1 Form I, Compound 1 Form II, or Compound 1 HCl Salt Form A were collected on a Bruker D8 DISCOVER powder diffractometer with a HI-STAR 2-dimensional detector and a flat graphite monochromator. A Cu sealed tube with Kα radiation was used at 40 kV, 35 mA. Samples were placed on silicon wafers with zero background at 25°C. For each sample, with 2 different θ 2 Angle Two data frames were collected at 120 seconds: 8° and 26°. Data were integrated using GADDS software and DIFFRACT plus EVA software merged. The reported uncertainty of the peak positions is ±0.2 degrees.
[0403] Jet Milling Description
[0404] Unmicronized Compound 1, Compound 1 Form I, Compound 1 Form II, or Compound 1 HCl Salt Form A was screened to remove lumps before it was placed in the jet mill hopper. All sieves are disposable, wipe clean before use. Using compressed nitrogen to control the feed ...
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