Production process of iron ion graphene based on multiphase quantum self-coupling reaction

A production process, phase quantum technology, applied in the field of iron ion graphene production process, can solve the problems of serious emissions, high energy consumption, etc., and achieve the effect of complete crystal lattice

Inactive Publication Date: 2018-07-10
天元羲王控股有限公司
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  • Abstract
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  • Claims
  • Application Information

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Problems solved by technology

Graphene oxide must be obtained first, and the emission is serious during the process, which consumes a lot of energy

Method used

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  • Production process of iron ion graphene based on multiphase quantum self-coupling reaction

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no. 1 example

[0025] refer to figure 1 , a kind of ferric ion graphene production technology based on heterogeneous quantum self-coupling reaction of the present invention, comprises the following steps:

[0026] S1. Feeding and mixing, input graphite powder and non-ionic additives successively into powder mixer and ribbon-screw-cone mixer to fully mix the three materials to obtain mixture A; the speed of powder mixer is 100-5000r / min, the stirring time is 10min; the stirring power of the ribbon-screw-conical mixer is 0.4kW / kg, and the stirring time is 20min;

[0027] S2. Preliminary reaction, transfer the mixture A to a quartz tube that can be repeatedly heated and cooled for repeated heating and cooling; the quartz tube is connected to the heating device and a low-temperature refrigerator to control the temperature rise and fall; the mixture A, a chelating wetting agent , The mass ratio of comprehensive impact agent and deionized water is 100000:1:1000:2000:100;

[0028] S3, further mi...

no. 2 example

[0032] A kind of ferric ion graphene production process based on heterogeneous quantum self-coupling reaction of the present invention comprises the following steps:

[0033] S1. Feeding and mixing, input graphite powder and non-ionic additives successively into powder mixer and ribbon-screw-cone mixer to fully mix the three materials to obtain mixture A; the speed of powder mixer is 100-5000r / min, the stirring time is 10min; the stirring power of the ribbon-screw-conical mixer is 0.4kW / kg, and the stirring time is 20min;

[0034] S2. Preliminary reaction, transfer the mixture A to a quartz tube that can be repeatedly heated and cooled for repeated heating and cooling; the quartz tube is connected to the heating device and a low-temperature refrigerator to control the temperature rise and fall; the mixture A, a chelating wetting agent , The mass ratio of comprehensive impact agent and deionized water is 100000:5:40000:2000:50000;

[0035] S3, further mixing, the mixture A, c...

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Abstract

The invention discloses a production process of iron ion graphene based on a multiphase quantum self-coupling reaction, wherein the production process includes the following steps: firstly, successively inputting a graphite powder and non-ionic auxiliary agents into a powder stirrer and a spiral ribbon screw conical mixer, and fully mixing the three materials, to obtain a mixture A; then, transporting the mixture A to a quartz tube which can perform repeated heating and cooling, and carrying out repeated heating and cooling treatment; next, inputting the mixture A, a chelating wetting agent, acomprehensive impact agent and deionized water into a liquid stirrer, and fully mixing to obtain a mixture B; then carrying out self-coupling reaction of the completely and evenly mixed mixture B ina multiphase quantum self-coupling reaction cylinder; and finally, transporting the final mixture having the self-coupling reaction completed into a vacuum degasser, vacuumizing, and then storing theproduct in a slurry storage cylinder. The high-purity graphene is non-oxidized graphene, and can be directly dispersed and applied.

Description

technical field [0001] The invention relates to the technical field of graphene application, in particular to a production process of iron ion graphene based on multiphase quantum self-coupling reaction. Background technique [0002] The application of graphene has attracted the attention of the whole world, but the research on graphene is still in its infancy. Graphene is a very unique two-dimensional new material. However, the application of this new material is mainly in the addition of materials. The development of deeper and functional materials is the direction of scientific and technological progress. This requires that raw materials must be materials with functional properties. The material made from the original graphene is called N-type graphene, which means that the current graphene material as an additive material does not have autonomous characteristics, and graphene without ions itself is called N-type graphene. The meaning of refers to: non-ionic graphene or...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01B32/19
CPCC01B2204/30
Inventor 梁思敬司徒若祺余朗生
Owner 天元羲王控股有限公司
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