Preparation method of textile finishing agent

A technology of textile finishing and thickening agent, applied in textile and papermaking, fiber treatment, physical treatment, etc., can solve the problems of poor bacteriostatic and washing resistance, and achieve the advantages of increased specific surface area, stable performance, and avoidance of phase separation. Effect

Inactive Publication Date: 2018-10-09
袁杰
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The technical problem to be solved by the present invention is to provide a preparation method of a textile finishing agent in view of the problem that the commonly used textile finishing agents are not strong in antibacterial and washable properties

Method used

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Examples

Experimental program
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Effect test

preparation example Construction

[0020] A preparation method of a textile finishing agent, comprising the steps of:

[0021] (1) Mix chitosan and sodium carbonate solution with a mass fraction of 20% according to the mass ratio of 1:10, stir at 220-250r / min for 30-40min, let stand at room temperature for 2-3h, and then place it at 70-80 ℃, at a speed of 300~350r / min, stir for 45~60min, cool to room temperature to obtain a chitosan solution, take the chitosan solution and add chitosan enzyme with 2% mass of the chitosan solution, at a temperature of 28~35 ℃, stirred and reacted at 400~450r / min for 2~3h, then inactivated the enzyme at 85~100℃ for 15~20min, cooled naturally to room temperature to obtain the feed liquid, and added the feed liquid with a mass ratio of 1:3~4 H with a score of 25% 2 o 2 Solution, mix evenly, soak for 2~3h to get the soaking solution;

[0022] (2) Take the soaking liquid and irradiate it with γ-rays for 10-15 minutes to obtain the irradiated matter. Take the irradiated matter by r...

Embodiment 1

[0027] Surfactant: Mix sodium lauryl ether sulfate and sodium dodecylbenzenesulfonate at a mass ratio of 1:1 to obtain a surfactant.

[0028] Thickener: mix carbomer, water, and polyisopropylene at a mass ratio of 1:50:0.5 to obtain a thickener.

[0029] Glycoprotein hydrolyzate: in parts by mass, take 30 parts of porcine serum albumin, 0.1 part of trypsin, and 100 parts of water, stir and enzymolyze at 25°C for 40 minutes, and inactivate the enzyme at 90°C for 15 minutes to obtain glycoprotein hydrolyzate.

[0030] A preparation method of a textile finishing agent, comprising the steps of:

[0031] (1) Mix chitosan and sodium carbonate solution with a mass fraction of 20% according to the mass ratio of 1:10, stir at 220r / min for 30min, let stand at room temperature for 2h, and then at 70°C, at a speed of 300r / min, Stir for 45 minutes, cool to room temperature to obtain chitosan solution, take chitosan solution and add chitosan enzyme with 2% mass of chitosan solution, at 28°...

Embodiment 2

[0037] Surfactant: Mix sodium lauryl ether sulfate and sodium dodecylbenzenesulfonate at a mass ratio of 1:1 to obtain a surfactant.

[0038] Thickener: Mix carbomer, water, and polyisopropylene at a mass ratio of 1:80:0.5 to obtain a thickener.

[0039] Glycoprotein hydrolyzate: in parts by mass, take 55 parts of porcine serum albumin, 0.4 part of trypsin, and 200 parts of water, stir and enzymolyze at 30°C for 60 minutes, and inactivate the enzyme at 110°C for 20 minutes to obtain glycoprotein hydrolyzate.

[0040] A preparation method of a textile finishing agent, comprising the steps of:

[0041] (1) Mix chitosan and sodium carbonate solution with a mass fraction of 20% according to the mass ratio of 1:10, stir at 250r / min for 40min, let stand at room temperature for 3h, and then at 80°C, at a speed of 350r / min, Stir for 60 minutes, cool to room temperature to obtain chitosan solution, take chitosan solution and add chitosan enzyme with 2% mass of chitosan solution, at 35...

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PUM

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Abstract

The invention discloses a preparation method of a textile finishing agent, and belongs to the field of chemical engineering. Carbomer dispersion liquid used as a thickener reacts with glycoprotein hydrolysate, and carbomer molecules can form hydrogen bonds together with a sugar residue on an oligosaccharide chain in a glycoprotein to generate a relatively strong mucus gel network structure achieving a thickening effect, so that the product stability is further improved; furthermore, the molecular structure of carbomer contains a large amount of carboxyl; after a part of the carboxy is neutralized, the carboxyl can be ionized; due to the mutual repulsion effect of negative charges, the carbomer molecules extend in a diffusing manner and is in an expanded state, so that physical crossing entanglement of a three-dimensional network structure in the system is realized; and meanwhile, the negative-charged carboxyl can shield positive charges in a part of the chitosan molecular structure toavoid excessive infiltration of a textile fiber, so that the bonding force is provided more stably, and the washability is improved. The preparation method solves the problem that the conventional textile finishing agent is low in antibacterial activity and washability at the present.

Description

technical field [0001] The invention belongs to the field of chemical industry, and in particular relates to a preparation method of a textile finishing agent. Background technique [0002] The functional finishing of textiles is a special finishing method that endows textiles with excellent properties such as use, safety, and appearance in order to meet certain special requirements for use of textiles. The functional finishing agent of textiles is a kind of product developed with the development of multidisciplinary technologies such as chemistry, biomedicine, polymer composite materials, photochemistry, thermodynamics, electricity, and ecology. Since the functional finishing of textiles is aimed at certain specific properties of textiles, it has strong purpose, good effect and high added value of the product. After functional finishing, textiles have a clear purpose and scope of use, and are also popular among consumers. According to statistics, the demand for functional...

Claims

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Application Information

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IPC IPC(8): D06M15/03D06M15/15D06M15/285D06M15/53D06M13/256D06M13/00D06M10/00
CPCD06M10/008D06M13/00D06M13/256D06M15/03D06M15/15D06M15/285D06M15/53D06M16/00
Inventor 袁杰陈炎刘红妹
Owner 袁杰
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