Preparation method of platinum-containing cube

A technology of a cube and a synthesis method, which is applied in the field of the preparation of platinum-containing cubes, can solve the problems of poor precision, complicated process flow of the preparation method of platinum-containing cubes, and no environmental protection.

Inactive Publication Date: 2018-11-02
程桂平
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] The preparation method of platinum-containing cubes in the prior art has complicated processes, poor precision, and is not environmentally friendly

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0015] A kind of synthetic method containing platinum cube, comprising:

[0016] Step 1: Add 10 mg potassium chloroplatinite, 6.6 mg, to a 25 mL high pressure reaction vial , 0.1mg copper chloride and 4.04g octadecylamine;

[0017] Step 2: Then add 0.1mL ethylene glycol to the above reaction vial with a pipette, raise the temperature to 160°C under 1atmCO atmosphere, and keep it for 3h;

[0018] Step 3: After cooling, add 15mL ethanol to the bottle and let it stand for 1h;

[0019] Step 4: pour off the upper layer solution, wash 2-3 times according to the above method, then transfer the product to a centrifuge tube and centrifuge with a mixed solvent of cyclohexane and ethanol to obtain an intermediate product;

[0020] Step 5: Add 13 mg of hexachloroplatinic acid, 6.6 mg of copper acetylacetonate, 20 mg of glucose, 2 mg of the intermediate product obtained in step 5, and 4.04 g of octadecylamine into a 25 mL high-pressure reaction flask;

[0021] Step 6: Then add 0.5mL of...

Embodiment 2

[0026] A kind of synthetic method containing platinum cube, comprising:

[0027] Step 1: Add 10 mg potassium chloroplatinite, 6.6 mg, to a 25 mL high pressure reaction vial , 0.2mg copper chloride and 4.04g octadecylamine;

[0028] Step 2: Then add 0.1mL ethylene glycol to the above reaction vial with a pipette, raise the temperature to 160°C under 1atmCO atmosphere, and keep it for 3h;

[0029] Step 3: After cooling, add 15mL ethanol to the bottle and let it stand for 1h;

[0030] Step 4: pour off the upper layer solution, wash 2-3 times according to the above method, then transfer the product to a centrifuge tube and centrifuge with a mixed solvent of cyclohexane and ethanol to obtain an intermediate product;

[0031] Step 5: Add 13 mg of hexachloroplatinic acid, 6.6 mg of copper acetylacetonate, 20 mg of glucose, 2 mg of the intermediate product obtained in step 5, and 4.04 g of octadecylamine into a 25 mL high-pressure reaction flask;

[0032] Step 6: Then add 0.5mL of...

Embodiment 3

[0037] A kind of synthetic method containing platinum cube, comprising:

[0038] Step 1: Add 10 mg potassium chloroplatinite, 6.6 mg, to a 25 mL high pressure reaction vial , 0.3mg copper chloride and 4.04g octadecylamine;

[0039] Step 2: Then add 0.1mL ethylene glycol to the above reaction vial with a pipette, raise the temperature to 160°C under 1atmCO atmosphere, and keep it for 3h;

[0040] Step 3: After cooling, add 15mL ethanol to the bottle and let it stand for 1h;

[0041] Step 4: pour off the upper layer solution, wash 2-3 times according to the above method, then transfer the product to a centrifuge tube and centrifuge with a mixed solvent of cyclohexane and ethanol to obtain an intermediate product;

[0042] Step 5: Add 13 mg of hexachloroplatinic acid, 6.6 mg of copper acetylacetonate, 20 mg of glucose, 2 mg of the intermediate product obtained in step 5, and 4.04 g of octadecylamine into a 25 mL high-pressure reaction flask;

[0043] Step 6: Then add 0.5mL of...

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PUM

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Abstract

The invention provides a synthesis method of a platinum-containing cube. The method comprises steps as follows: step 1, 10 mg of potassium tetrachloroplatinate, 6.6 mg of a compound shown in the description, 0.1 mg of copper chloride and 4.04 g of octadecylamine are added to a 25 mL high-pressure reaction flask; step 2, 0.1 mL of ethanediol is added to the reaction flask by a pipette, and a mixedsolution is heated to 160 DEG C under the latmCO atmosphere and is kept at the temperature for 3 h.

Description

technical field [0001] The invention relates to a preparation method of a platinum-containing cube. Background technique [0002] The preparation method of platinum-containing cubes in the prior art has complicated process, poor precision and is not environmentally friendly. Contents of the invention [0003] A kind of synthetic method containing platinum cube, comprising: [0004] Step 1: Add 10 mg potassium chloroplatinite, 6.6 mg, to a 25 mL high pressure reaction vial , 0.1mg copper chloride and 4.04g octadecylamine; [0005] Step 2: Then add 0.1mL ethylene glycol to the above reaction vial with a pipette, raise the temperature to 160°C under 1atmCO atmosphere, and keep it for 3h; [0006] Step 3: After cooling, add 15mL ethanol to the bottle and let it stand for 1h; [0007] Step 4: pour off the upper layer solution, wash 2-3 times according to the above method, then transfer the product to a centrifuge tube and centrifuge with a mixed solvent of cyclohexane and ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07F15/00B22F9/24
CPCC07F15/0086B22F9/24
Inventor 程桂平
Owner 程桂平
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