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Continuous production device for aminated graphene and method

A technology of aminated graphene and production methods, which is applied in the direction of chemical instruments and methods, inorganic chemistry, carbon compounds, etc., can solve the problems that remain in industrialized large-scale production, and achieve the improvement of reaction efficiency, equipment efficiency, The effect of small diameter

Active Publication Date: 2018-11-13
CHANGZHOU HIGHBERY NEW NANO MATERIALS TECH CO LTD +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

In the prior art, the preparation of aminated graphene is still in the laboratory stage, and industrialized large-scale production has not yet been realized. The problem to be solved is how to continuously and stably produce high-quality aminated graphene in the industry

Method used

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  • Continuous production device for aminated graphene and method

Examples

Experimental program
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Effect test

Embodiment 1

[0032] A kind of continuous production device of graphene amide of the present embodiment, such as figure 1 As shown, it includes acid treatment device 1, oxidation device 2, first washing suction filtration device 3, second washing suction filtration device 4, dispersion treatment device 5, first homogenization treatment device 6, first microreaction device connected in sequence 7. The first tubular reaction device 8, the second tubular reaction device 9, the first suction filtration and redispersion device 10, the second micro-reaction device 11, the third tubular reaction device 12, the fourth tubular reaction device 13, The second suction filtration and redispersion device 14, the third suction filtration and redispersion device 15, the first reaction product storage tank 16, the second homogenization treatment device 17, the third homogenization treatment device 18 and the second reaction product storage tank 19. A first raw material high-level addition device 607 is prov...

Embodiment 2

[0060] The present embodiment adopts the same device as in Example 1 to carry out the continuous production of graphene amide, which comprises the following steps:

[0061] Step 1, add 10kg of graphite powder to 10kg of dilute hydrochloric acid (mass fraction 15%), soak it at 20°C, and transport it to the oxidation device 2 at a speed of 100kg / h by a pump after 0.5h, and add it through an online addition system. 100kg main oxidant and 10kg co-oxidant, the main oxidant potassium perchlorate is added at a rate of 5kg / h, and the addition rate of the co-oxidant peroxyester is 2kg / h, and the temperature is controlled at 80 ° C. After 10 hours of reaction, it is pumped to the first washing pump. The filter device 3 is repeatedly washed with deionized water and suction filtered three times, and then N,N-dimethylformamide is added for dispersion, and the material is transported into the second washing and suction filter device 4 by a pump, and the N,N-di After methylformamide washing ...

Embodiment 3

[0072] The present embodiment adopts the same device as in Example 1 to carry out the continuous production of graphene amide, which comprises the following steps:

[0073] Step 1, 10kg graphite powder was added to 20kg oxalic acid, soaked at 10°C, transported to oxidation device 2 by a pump at a speed of 100kg / h after 2 hours, and 10kg main oxidant and 1kg pro-oxidant were added through the online addition system, The addition rate of the main oxidant potassium dichromate is 5kg / h, the addition rate of the auxiliary oxidant peroxycarbonate is 2kg / h, and the temperature is controlled at 60 ° C. Deionized water is repeatedly washed and suction filtered for three times, then N,N-dimethylformamide is added for dispersion, and the material is transported into the second washing and suction filtration device 4 by a pump, and washed with N,N-dimethylformamide , After three times of suction filtration, graphite oxide is dispersed in N,N-dimethylformamide to obtain graphite oxide slur...

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Abstract

The invention discloses a continuous production device for aminated graphene and a method and belongs to the technical field of graphene preparation. The continuous production device comprises an acidtreatment device, an oxidation device, a first washing suction filtration device, a second washing suction filtration device, a dispersion treatment device, a first homogenization treatment device, afirst micro-reaction device, a first tubular reaction device, a second tubular reaction device, a first suction filtration and dispersion device, a second micro-reaction device, a third tubular reaction device, a fourth tubular reaction device, a second suction filtration and dispersion device, a third suction filtration and dispersion device, a first reaction product storage tank, a second homogenization treatment device, a third homogenization treatment device and a second reaction product storage tank; a static mixer is arranged inside a material conveying tube. Modified aminated grapheneproduced by using the device is small in piece size, narrow in piece diameter distribution, high in single layer rate, free of pollution in a production process, and a raw material base is provided for on-scale application of the aminated graphene.

Description

technical field [0001] The invention belongs to the technical field of graphene preparation, and more particularly, relates to a continuous production device and method of aminated graphene. Background technique [0002] Graphene is a carbon atom with sp 2 The hybrid orbitals form a hexagonal flat film with a honeycomb lattice, with a thickness of one carbon atomic layer (0.35 nm), which has excellent mechanical, electrical and thermal properties. At present, graphene is widely used in the composite modification of materials. Using the excellent properties of graphene to modify the matrix material can significantly improve the performance of the matrix material. Therefore, graphene nanocomposites have become a hot research topic in the material field. [0003] In order to ensure the interface between graphene and the matrix material, the surface of graphene needs to be modified by small molecules to achieve the purpose of introducing groups on the surface of graphene. For e...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01B32/194
CPCC01B32/194
Inventor 梁燕曹建鹏蒋炎黄荣庆
Owner CHANGZHOU HIGHBERY NEW NANO MATERIALS TECH CO LTD
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