A method for efficiently utilizing high-alumina coal gangue
A high-alumina coal gangue, high-efficiency technology, applied in chemical instruments and methods, aluminum compounds, silica, etc., can solve problems such as unseen reports
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Embodiment 1
[0032] (1) if figure 1 As shown, the analysis results of coal gangue raw materials and ash content are shown in Table 1.1. It can be seen from the table that this coal gangue has a relatively high calorific value, and the heat should be recovered before slag utilization;
[0033] Table 1.1 Coal gangue raw material and ash analysis
[0034]
[0035] (2) Dried the coal gangue and pulverized it, and ground it to a sieve residue of 9.98% through an 80-mesh sieve, and used a circulating fluidized bed to recover heat to obtain slag;
[0036] (3) Add industrial sulfuric acid with a mass concentration of 98% to the coal gangue slag of step (2) at a mass ratio of 1:1.2 to gangue, and solidify at 50°C;
[0037] (4) According to the mass ratio of industrial sulfuric acid and slag being 0.2, take out the coal gangue solidified material in step (3) and add 98% industrial sulfuric acid in the form of spray, and transfer it to a vertical acidification kiln for acidification reaction. Th...
Embodiment 2
[0044] (1) The analysis results of coal gangue raw materials and ash content are shown in Table 2.1. It can be seen from the table that the low-level calorific value of this coal gangue is 820cla / kg, which meets the heat recovery requirements. The heat should be recovered before slag utilization;
[0045] Table 2.1 Coal gangue raw material and ash analysis
[0046]
[0047] (2) Dried the coal gangue and pulverized it, and ground it to a sieve residue of 6.23% through an 80-mesh sieve, and used a circulating fluidized bed to recover heat to obtain slag;
[0048] (3) adding industrial sulfuric acid with a mass concentration of 98% to the coal gangue slag of step (2) at a mass ratio of 1:1.1 to gangue, and solidifying at room temperature;
[0049] (4) According to the mass ratio of industrial sulfuric acid and slag being 0.1, take out the coal gangue solidified material in step (3) and add 98% industrial sulfuric acid in the form of spray, and transfer it to a vertical acidifi...
Embodiment 3
[0056] (1) The analysis results of coal gangue raw materials and ash content are shown in Table 3.1. It can be seen from the table that the low-level calorific value of this coal gangue is 452cla / kg, which does not meet the heat recovery requirements. The coal gangue is directly used after drying, crushing and grinding;
[0057] Table 3.1 Coal gangue raw material and ash analysis
[0058]
[0059] (2) Grinding the coal gangue in step (1) to a sieve residue of 4.56% through a 100-mesh sieve;
[0060] (3) Add industrial sulfuric acid with a mass concentration of 98% to the coal gangue slag of step (2) at a mass ratio of 1:1.2 to gangue, and solidify at 35°C;
[0061] (4) According to the mass ratio of industrial sulfuric acid and slag being 0.15, take out the coal gangue solidified material in step (3) and add 98% industrial sulfuric acid in the form of spray, and transfer it to a vertical acidification kiln for acidification reaction. The heating temperature at the inlet of...
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