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Device and method for slag metal high-temperature reaction experiment study in metallurgical process

A technology for high-temperature reaction and experimental research, which is applied in the field of devices for experimental research on slag-gold high-temperature reaction in metallurgical processes, can solve the problems of molten steel or molten slag erosion, uncertainty, high temperature reaction temperature of slag blowing, and achieves low price, The effect of low experiment cost, convenient and fast experiment

Active Publication Date: 2019-01-01
NORTHEASTERN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] Aiming at the problems existing in the current high-temperature reaction experiment of slag-gold in the metallurgical process, the present invention provides a device and method for experimental research on the high-temperature reaction of slag-gold in the metallurgical process, which solves the problem of molten steel or molten slag corroding the crucible in the high-temperature experiment. The problem of material being blown away and the problem of uncertain high-temperature reaction temperature, and multi-stage multiple sampling is used to study the thermodynamics of high-temperature reaction when necessary

Method used

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  • Device and method for slag metal high-temperature reaction experiment study in metallurgical process
  • Device and method for slag metal high-temperature reaction experiment study in metallurgical process
  • Device and method for slag metal high-temperature reaction experiment study in metallurgical process

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Embodiment 1

[0041] The slag used in this example was prepared with analytically pure chemical reagents. The specific components and their mass percentages are shown in Table 1. The steel material is GCr15 bearing steel, and the specific components are shown in Table 2.

[0042] Table 1 The chemical composition of the slag used in the experiment

[0043]

[0044] In this embodiment, 50 g of slag and 500 g of steel are used, and the reaction temperature of slag and gold is 1600° C.

[0045] This embodiment adopts figure 1 The experimental steps of the device in the metallurgical process slag-gold high-temperature reaction experiment are as follows:

[0046] Step 1: At room temperature, put the graphite jacketed crucible, graphite support frame and magnesium oxide crucible with steel material into the heating furnace in sequence according to the structure of the experimental device;

[0047] Step 2: Raise the temperature of the heating furnace. When the temperature of the heating furnac...

Embodiment 2

[0054] The slag used in this example was prepared with analytically pure chemical reagents. The specific components and mass percentages are shown in Table 3. The steel material is M2 high-speed steel, and the specific components are shown in Table 4. The added deoxidizer is rare earth magnesium alloy.

[0055] Table 3 The chemical composition of the slag used in the experiment

[0056]

[0057] In this embodiment, 100 g of slag and 500 g of steel are used, and the reaction temperature of slag and gold is 1500° C.

[0058] This embodiment adopts figure 1 The specific experimental steps for the high-temperature reaction experiment of slag-gold in the metallurgical process are as follows:

[0059] Step 1: At room temperature, put the graphite jacketed crucible, graphite support frame and magnesium oxide crucible with steel material into the heating furnace in sequence according to the structure of the experimental device;

[0060] Step 2: Raise the temperature of the heati...

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Abstract

The invention belongs to the field of high-temperature metallurgy experiments and relates to a device and method for a slag metal high-temperature reaction experiment in the metallurgical process. Theexperimental device comprises a supporting device, a hanging device, a magnesia crucible, a material adding molybdenum hook and L-shaped iron pieces, wherein the supporting device is composed of a graphite outer sleeve crucible and a graphite supporting rack, the graphite supporting rack is movably fixed on the graphite outer sleeve crucible, the graphite outer sleeve crucible is internally provided with the magnesia crucible, a pi-shaped hook is provided with a sunk molybdenum wire which is horizontally arranged on the graphite supporting rack and passes the circle center of the graphite supporting rack, one other V-shaped molybdenum wire is connected with the sunk position of the horizontal molybdenum wire in a lapped manner, and the bottom faces of the L-shaped iron pieces are larger than a centre hole and are arranged inside the graphite crucible for blocking the centre hole in the bottom of the graphite crucible. By means of the device for the slag metal high-temperature reactionexperiment in the metallurgical process, multiple sampling can be performed after steel materials are melted and before slag materials are added, after slag metals react for a certain time and aftera deoxidizing agent is added in according to requirements in the high-temperature experiment, and the experiment is performed more conveniently and efficiently.

Description

technical field [0001] The invention belongs to the field of high-temperature metallurgical experiments, and relates to a device and method for experimental research on slag-gold high-temperature reaction in metallurgical processes. Background technique [0002] In recent years, with the advancement of domestic steelmaking technology and the continuous improvement of the research and development level of high-quality steel, the requirements for the control of non-metallic inclusions in steel have become more and more stringent. The production of clean steel with high efficiency and low cost is an important technology in the field of iron and steel at home and abroad, and the control of non-metallic inclusions in steel is the key to the production of clean steel, and it is also a research hotspot in the field of iron and steel metallurgy. The non-metallic inclusions in the steel destroy the continuity of the steel matrix, and have adverse effects on the ductility, toughness, ...

Claims

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Application Information

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IPC IPC(8): F27B17/02
CPCF27B17/02
Inventor 董艳伍柏川姜周华侯志文曹海波李毓硕
Owner NORTHEASTERN UNIV
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