Method for preparing composite metal surface anti-rusting detergent

A rust-removing cleaning agent and a technology for metal surfaces, applied in the field of metal surface cleaning, can solve problems such as troublesome use and operation, corrosion of metal surfaces, complex composition, etc., and achieve the effects of easy industrial production, easy control of conditions, and simple preparation process.

Inactive Publication Date: 2019-01-04
UNIV OF JINAN
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

This patented composition produces an effective solution that can remove dirt from metals without causing damage or harm their properties during use. It also provides safety features while being produced at lower costs compared to existing methods like chemical treatment techniques.

Problems solved by technology

This patents discusses different ways that may help protect metals from being damaged over their lifetimes without causing any harm during storage or usage. One way involves applying coatings made up mostly of organisms called rust (a type of bacteria) onto the surfaces where these coats form insoluble layers known collectively referred to herein as “rust”). These deposits gradually deteriorate through exposure to moist environments such as rainwater, resulting in reduced durability of the metal. To address this problem, antirritants like calcium chlorite were developed instead of traditional acquirements involving solvents. Another approach was found to involve chemically treating the metal before adding them into solutions containing nitric acid or sulfur dioxides.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0016] (1) Preparation of liquid A: add ethanol: 700mL, phosphoric acid: 240mL respectively into the reactor, stir well, react for 7 hours, leave overnight to obtain liquid A;

[0017] (2) Preparation of liquid B: Into the reactor, add water: 630 mL, sodium cyclohexanediamine tetraacetate: 15g, tetradecyl dihydroxyethylamine oxide: 15g, trifluoroacetic acid: 60g, bromide 1-heptyl-3 methylimidazole: 150g, triisopropanolamine: 130 mL, stir and dissolve to obtain liquid B;

[0018] (3) Preparation of composite metal surface derusting and cleaning agent: In the reactor, mix liquid A and liquid B at a volume ratio of 1:1 at a speed of 250 rpm and stir for 60 minutes to obtain a composite metal surface derusting agent detergent.

Embodiment 2

[0020] (1) Preparation of liquid A: add ethanol: 670mL, phosphoric acid: 250mL respectively into the reactor, stir well, react for 6 hours, leave overnight to obtain liquid A;

[0021] (2) Preparation of liquid B: Into the reactor, add water: 600 mL, sodium cyclohexanediamine tetraacetate: 20g, tetradecyl dihydroxyethylamine oxide: 20g, trifluoroacetic acid: 80g, bromide 1-heptyl-3 methylimidazole: 160g, triisopropanolamine: 120 mL, stir and dissolve to obtain liquid B;

[0022] (3) Preparation of composite metal surface derusting and cleaning agent: In the reactor, mix liquid A and liquid B at a volume ratio of 1:1 at a speed of 250 rpm and stir for 50 minutes to obtain a composite metal surface derusting agent detergent.

Embodiment 3

[0024] (1) Preparation of liquid A: add ethanol: 720mL, phosphoric acid: 230mL respectively into the reactor, stir well, react for 8 hours, leave overnight to obtain liquid A;

[0025] (2) Preparation of liquid B: Into the reactor, add water: 660 mL, sodium cyclohexanediamine tetraacetate: 10 g, tetradecyl dihydroxyethyl amine oxide: 10 g, trifluoroacetic acid: 40 g, bromide 1-heptyl-3 methylimidazole: 130g, triisopropanolamine: 150 mL, stir and dissolve to obtain liquid B;

[0026] (3) Preparation of composite metal surface derusting and cleaning agent: In the reactor, mix liquid A and liquid B at a volume ratio of 1:1 at a speed of 250 rpm, and stir for 70 minutes to obtain a composite metal surface derusting agent detergent.

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PUM

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Abstract

The invention discloses a method for preparing a composite metal surface anti-rusting detergent. The method is characterized by comprising the following steps: putting the following components in percentage by mass into a reactor: 53-57% of ethanol, and 43-47% of phosphoric acid so as to obtain a liquid A; putting the following components in percentage by mass into the reactor: 60-66% of water, 1.0-2.0% of sodium cyclohexanediamine tetraacetic acid, 1.0-2.0% of tetradecyl diethoxy amine oxide, 4-8% of trifluoroacetic acid, 13-17% of bromination-1-heptyl-3-methyl imidazole and 12-15% of tri-isopropanolamine, and stirring and dissolving so as to obtain a liquid B; stirring the liquid A and the liquid B for 50-70 minutes in a volume ratio of 1:1 at a rotation speed of 250rpm, thereby obtaining the composite metal surface anti-rusting detergent. No acid mist is generated from the detergent and a cleaning waste liquid, iron structures are not corroded, and meanwhile, the detergent has corrosion resistance, is capable of preventing secondary rusting and is safe and environmental-friendly.

Description

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Claims

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Application Information

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Owner UNIV OF JINAN
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