A separation process of petroleum associated gas
A technology for petroleum associated gas and associated gas, which is applied in the petroleum industry, separation methods, semi-permeable membrane separation, etc., can solve the problems of high cost, inability to condense methane, complicated and complicated devices, etc., and achieves improved efficiency, high selectivity, and separation. fast effect
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Embodiment 1
[0027] Embodiment 1: the preparation one of composite film:
[0028] This embodiment is to prepare the composite membrane used in the membrane separation step of the petroleum associated gas separation process, first prepare the gel filtration layer of the middle layer:
[0029] The lead-silver alloy plate is used as the anode, and the rolled aluminum plate wrapped with a conductive sponge with a porosity of 60% is used as the cathode, and they are suspended in a zinc sulfate solution in parallel, and a 12V direct current is applied. When the elemental zinc fills the gap of the sponge, the electrolysis ends. Take out the sponge, soak it in a glycerin-ethanol solution with a glycerin concentration of 15wt% for 3 hours, place it in an oven at 60°C for 1 hour, and then put it in a muffle furnace at 250°C for 80 minutes, take it out, and use a deionized Wash it with water, dry it, and chop it to get a spongy skeleton;
[0030] The sponge-like skeleton is prepared by electro-depos...
Embodiment 2
[0037] Embodiment 2: the preparation two of composite film:
[0038] This embodiment is to prepare the composite membrane used in the membrane separation step of the petroleum associated gas separation process, first prepare the gel filtration layer of the middle layer:
[0039] The lead-silver alloy plate is used as the anode, and the rolled aluminum plate wrapped with a conductive sponge with a porosity of 70% is used as the cathode, and they are suspended in the zinc sulfate solution in parallel, and 12V DC is applied. When the elemental zinc fills the gap of the sponge, the electrolysis ends. Take out the sponge, soak it in a glycerin-ethanol solution with a glycerol concentration of 20wt% for 3 hours, place it in an oven at 55°C for 2 hours, and then place it in a muffle furnace at 300°C for 60 minutes and take it out, and use a deionized Wash it with water, dry it, and chop it to get a spongy skeleton;
[0040] Dissolve 40 g of 1-butyl-3-vinylimidazole bromide in 300 ml o...
Embodiment 3
[0044] Example 3: Preparation of composite membrane Three:
[0045] The present embodiment is to prepare a composite membrane for the membrane separation step of the oil-associated gas separation process. First, the gel filtration layer of the intermediate layer is prepared:
[0046] The lead-silver alloy plate is used as the anode, and the rolled aluminum plate wrapped with the conductive sponge with porosity of 80% is used as the cathode. It is suspended in a zinc sulfate solution in parallel, and 12V DC is applied. When the elemental zinc fills the sponge gap, the electrolysis ends. The sponge was taken out, soaked in a glycerol-ethanol solution with a glycerin concentration of 25wt% for 4 hours, placed in an oven at 50°C for 2 hours, and then placed in a muffle furnace at 350°C for 50 minutes and then taken out. After washing with water, dry it, and chop it up to obtain a spongy skeleton;
[0047] Dissolve 40 g of 1-butyl-3-vinylimidazole bromide in 300 ml of acetonitrile...
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Abstract
Description
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Application Information
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