Quality control method and equipment for traditional Chinese medicine decoction piece processing
A quality control method and the technology of Chinese herbal pieces, which are applied in the direction of making medicines into special physical or taking forms, using material absorption weighing, measuring devices, etc., can solve the problem of accurately determining the content of index components of Chinese herbal pieces, etc. problem, to achieve the effect of realizing quick judgment, ensuring consistency and stability
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Embodiment 1
[0030] This embodiment provides a kind of equipment for processing Chinese herbal decoction pieces, such as figure 1 As shown, it includes a processing tank 1 and a circulation pipeline 2. The circulation pipeline 2 is arranged outside the processing tank 1 and communicates with the upper and lower ends of the processing tank 1. The processing tank 1 is connected with a hopper 11 and a liquid outlet. The circulation pipeline 2 is provided with a detection tank 4 and a circulation pump 3 connected with the circulation pipeline 2 from top to bottom, and the circulation pump 3 is connected with the bottom of the processing tank 1 through the first liquid outlet valve 18 to detect A detection probe 5 is installed in the pool 4, and the detection probe 5 communicates with the spectrum analyzer 6. The spectrum analyzer 6 stores component detection models of the processed solutions of various Chinese medicinal materials, and the spectral information of the processed solutions in the d...
Embodiment 2
[0037] This embodiment provides a quality control method for processing traditional Chinese medicine decoction pieces using the equipment of Embodiment 1. Taking the processing of Aconitum aconitum as an example: Aconitum aconitum is the dried mother root of the plant Aconitum ranunculaceae, which is highly toxic, and the main toxic substance is diester Aconitine (C 34 h 47 NO 11 ), Hypoaconitine (C 33 h 45 NO 10 ) and neoaconitine (C 33 h 45 NO 11 )) total content T c Not more than 0.040%, that is, not more than 400μg / g, the hydrolysis product of diester-type alkaloids-benzoylaconitine (C 32 h 45 NO 10 ), benzoyl aconitine (C 31 h 43 NO 9 ) and benzoyl neoaconitine (C 31 h 43 NO 10 ) of the total content T b It should be 0.070% to 0.15%; the specific quality control method is as follows:
[0038] 1. Take the manually selected clean Aconitum aconitum, and detect the content of the toxic substance diester alkaloids in it. Based on the dried Aconitum aconitum, ...
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