Preparation method of continuous aroma enhancement type solid aromatic bead for cigarette

A tobacco flavoring and solid state technology is applied in the field of preparation of continuous aromatizing solid incense beads for cigarettes, which can solve the problems that the incense beads cannot provide users with a uniform and stable aromatizing experience, residues, and poor aromatizing effects, and achieves continuous and stable aromatization. The effect of incense experience

Inactive Publication Date: 2019-06-14
CHINA TOBACCO JIANGXI IND CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The types of fragrant beads include microcapsules, quick-fried beads, dripping pills, and powdery granules, and the molding methods vary according to their shapes. However, during the preparation process of quick-fried beads and dripping pills, some exogenous harmful ingredients are easily added, such as: low molecular weight Aldehydes and ketones, such as formaldehyde and acetaldehyde, benzene series, plasticizers, etc., may remain in the fragrance beads and cause potential harm to the human body; while powder particles are usually too small in size, consumers are likely to have safety concerns
At present, there is an existing technology of using zeolite, biochar, cyclodextrin and other materials to make large-particle solid flavor beads, and the inherent porous adsorption structure of zeolite and other materials is used to absorb and store flavor components. During the smoking process of cigarettes, flavor components It will be taken out by the mainstream smoke with the inhalation, and then perceived by the smoker. However, most of the aroma components are still trapped in the filter, and the retention rate is as high as 75%, while only 5% to 10% Fragrance components will be transferred to the mainstream smoke, and usually the aroma components are affected by heat and the user’s smoking habits are different, they will overflow concentratedly in the early stage of smoking, and the effect of increasing fragrance in the later stage of smoking is poor. During the whole smoking process, the fragrance beads cannot Provide users with a uniform and stable fragrance enhancement experience

Method used

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  • Preparation method of continuous aroma enhancement type solid aromatic bead for cigarette
  • Preparation method of continuous aroma enhancement type solid aromatic bead for cigarette

Examples

Experimental program
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Effect test

Embodiment 1

[0039] (1) Add 10g of soybean lecithin to 20 times the weight of absolute ethanol, stir at 45°C, and the stirring speed is 1000r / min. After the dissolution is complete, slowly add 100g of peppermint oil and 150g of 20% Tween 80 solution, and continue stirring 45min, obtain emulsion;

[0040] (2) Add 200g of ethyl cellulose (90mPa·s) to the emulsion, keep stirring at 45°C for 30min at a stirring speed of 800r / min, let cool and add 80g of hydroxypropylmethylcellulose (3000mPa·s ), continue to stir for 1h, then concentrate the solution in vacuum to one-third of the original volume, and obtain a slow-release powder after spray drying;

[0041] (3) Mix the slow-release powder with cellulose acetate and carboxymethyl cellulose at a weight ratio of 1:2.5:0.8, add an appropriate amount of water and use an extruder for secondary granulation, and obtain solid fragrance beads after drying.

Embodiment 2

[0043] (1) Add 5g of soybean lecithin to 20 times the weight of absolute ethanol, stir at 45°C, and the stirring speed is 1000r / min. After the dissolution is complete, slowly add 100g of peppermint oil and 50g of 20% Tween 80 solution, and continue stirring 45min, obtain emulsion;

[0044] (2) Add 250g of ethyl cellulose (70mPa·s) to the emulsion, keep stirring at 45°C for 30min at a stirring speed of 800r / min, let cool and add 200g of hydroxypropylmethylcellulose (4000mPa·s ), continue to stir for 2h, then concentrate the solution in vacuum to 1 / 4 of the original volume, and obtain a slow-release powder after spray drying;

[0045] (3) Mix the slow-release powder with cellulose acetate and carboxymethyl cellulose at a weight ratio of 1:2.5:0.8, add an appropriate amount of water and use an extruder for secondary granulation, and obtain solid fragrance beads after drying.

Embodiment 3

[0047](1) Add 8g of egg yolk lecithin to 20 times the weight of absolute ethanol, stir at 50°C, and the stirring speed is 1000r / min, after the dissolution is complete, slowly add 100g of peppermint oil and 100g of 20% Tween 80 solution, and continue stirring 50min, obtain emulsion;

[0048] (2) Add 300g of ethyl cellulose (55mPa·s) to the emulsion, keep stirring at 45°C for 30min at a stirring speed of 800r / min, let cool and add 150g of hydroxypropylmethylcellulose (5000mPa·s ), continue to stir for 2h, then concentrate the solution in vacuum to one-third of the original volume, and obtain a slow-release powder after spray drying;

[0049] (3) Mix the slow-release powder with cellulose acetate and carboxymethyl cellulose at a weight ratio of 1:2.5:0.8, add an appropriate amount of water and use an extruder for secondary granulation, and obtain solid fragrance beads after drying.

[0050] Weigh the same weight of solid incense beads prepared in Comparative Examples and Example...

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Abstract

The invention discloses a preparation method of a continuous aroma enhancement type solid aromatic bead for a cigarette. The preparation method comprises the following steps that (1) lecithin is addedto absolute ethyl alcohol, stirring is carried out at 45-50 DEG C, after complete dissolution, cigarette flavor and a 20% tween 80 solution are slowly added, stirring is continued for 30-45 min, andemulsion liquid is obtained; (2) ethyl cellulose is added to the emulsion liquid, stirring is continued for 30-45 min, hydroxypropyl methyl cellulose is added after a mixture is cooled, stirring is continued for 1-2 h, the volume of a solution is subjected to vacuum concentration to one third to one fourth of the original volume, and slow releasing powder is obtained through spray drying; and (3)the slow releasing powder is mixed with cellulose acetate and carboxymethyl cellulose, secondary granulation is carried out, and the solid aromatic bead is obtained after drying. According to the preparation method of the continuous aroma enhancement type solid aromatic bead for the cigarette, when the prepared solid aromatic bead is used, the retention rate of aromatic components in a filter is low, the aromatic compositions can be transferred to a mainstream smoke particle phase continuously and stably, and a user can obtain uniform and stable aroma enhancement experience.

Description

technical field [0001] The invention belongs to the technical field of tobacco production, and in particular relates to a method for preparing continuous flavor-increasing solid flavor beads for cigarettes. Background technique [0002] In recent years, with the emergence of composite multi-element filter sticks and the development trend of cigarette tar reduction and harm reduction, in order to make up for the resulting loss of smoke aroma, more and more brands have begun to use the "flavor bead addition" technology as an auxiliary flavoring The method, fragrance beads, is one or more flavor capsules, granules or microbeads added to the cigarette tip, which can realize the artificial and controllable release of characteristic fragrance during the smoking process of cigarettes, and reduce the influence of the external environment on smoking flavor and the loss of flavor caused by it, enrich the taste of cigarette smoking, and realize the moisturizing and flavor enhancement i...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/00A24D3/04
Inventor 蔡继宝苏加坤罗海涛徐达郭磊何力任周营邵灯寅钟宇生徐振宇
Owner CHINA TOBACCO JIANGXI IND CO LTD
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