Unlock instant, AI-driven research and patent intelligence for your innovation.

A deformation heat treatment process for improving the intergranular corrosion resistance of austenitic stainless steel

A technology of austenitic stainless steel and deformation heat treatment, which is applied in the field of deformation and heat treatment of metal materials to achieve uniform deformation and excellent intergranular corrosion resistance

Active Publication Date: 2020-08-28
HUAIHAI INST OF TECH
View PDF4 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In fact, uniaxial tensile deformation is generally used to test the mechanical properties of materials, such as yield strength, tensile strength, elongation, etc. There are also a few concepts based on grain boundary engineering that use uniaxial tensile deformation to optimize the distribution of grain boundary characteristics of materials. However, there is no report on the use of cross tensile deformation combined with annealing to control the distribution of grain boundary characteristics of austenitic stainless steel, thereby improving the intergranular corrosion resistance of austenitic stainless steel

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • A deformation heat treatment process for improving the intergranular corrosion resistance of austenitic stainless steel
  • A deformation heat treatment process for improving the intergranular corrosion resistance of austenitic stainless steel
  • A deformation heat treatment process for improving the intergranular corrosion resistance of austenitic stainless steel

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] Cross tensile deformation of austenitic stainless steel rods or pipes (such as figure 1 Shown), the cross tensile deformation is 3%, 7%, 14%, 21%. Subsequently, the deformed sample was annealed at 1050°C for 5 minutes in a heat treatment furnace, and then taken out for water quenching after heat preservation. The specific process parameters are shown in Table 2. The proportion of low ΣCSL inside the sample after deformation heat treatment changes with the change of cross tensile deformation. The specific test results are shown in Table 2.

[0033] The samples after deformation heat treatment were inlaid with epoxy resin and curing agent to prepare standard electrochemical corrosion samples. at room temperature in 0.5M H 2 SO 4 Potentiodynamic reactivation (EPR) experiments and polarization curve measurements were carried out on the samples in +0.01M KSCN solution. The reactivation current ratio and self-corrosion potential changed with the change of cross tensile def...

Embodiment 2

[0037] Cross tensile deformation of austenitic stainless steel rods or pipes (such as figure 1 Shown), the amount of cross tensile deformation is selected as 5%. Subsequently, the deformed samples were annealed in a heat treatment furnace. The annealing temperatures were 1000°C, 1050°C, 1100°C and 1150°C respectively, and the annealing time was 5 minutes. After deformation heat treatment, the low ΣCSL ratio inside the sample changes with the annealing temperature. The specific test results are shown in Table 3.

[0038]The samples after deformation heat treatment were inlaid with epoxy resin and curing agent to prepare standard electrochemical corrosion samples. at room temperature in 0.5M H 2 SO 4 Potentiodynamic reactivation (EPR) experiments and polarization curve measurements were performed on the samples in +0.01M KSCN solution. The reactivation current ratio and self-corrosion potential changed with the annealing temperature. Table 3 lists the reactivation current ra...

Embodiment 3

[0043] Use an electronic tensile testing machine to carry out cross tensile deformation on austenitic stainless steel rods or pipes, and the amount of cross tensile deformation is selected as 5%. Subsequently, the deformed samples were annealed in a heat treatment furnace. The annealing temperature was 1050°C, and the annealing time was 5 min, 10 min, and 30 min. The low ΣCSL ratio inside the sample after deformation heat treatment changes with the annealing time. The specific test results are shown in Table 4.

[0044] The samples after deformation heat treatment were inlaid with epoxy resin and curing agent to prepare standard electrochemical corrosion samples. at room temperature in 0.5M H 2 SO 4 Potentiodynamic reactivation (EPR) experiments and polarization curve measurements were performed on the samples in +0.01M KSCN solution. The reactivation current ratio and self-corrosion potential changed with the annealing time. Table 4 lists the reactivation current ratio and...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention relates to an ausforming technology method for improving austenitic stainless steel intercrystalline corrosion resistance performance. Firstly, solution treatment is conducted on an austenitic stainless steel alloy, then after solid treatment, the alloy is treated with cross tensile deformation, the total amount of cross tensile deformation is controlled at 3% to 21%, the sub-tensiledeformation amount is 1.5% to 10.5%, finally, the cross-tensile deformed material is placed in a heat treatment furnace and is subjected to heat preservation for 5 min to 30 min under 1000 DEG C to 1200 DEG C, and after heating, a sample is quickly put into an ice water mixture for water quenching treatment. Control over characteristic distribution of austenitic stainless steel can be realized, and thus the corrosion resistance performance of the austenitic stainless steel is significantly improved.

Description

technical field [0001] The invention relates to the technical field of metal material deformation and heat treatment technology, in particular to a deformation heat treatment process method for improving the anti-intergranular corrosion performance of austenitic stainless steel. Background technique [0002] Austenitic stainless steel has excellent mechanical properties and good corrosion resistance under normal conditions, and is widely used in industries such as petroleum, chemical industry and power stations. However, during the use of austenitic stainless steel, leakage accidents caused by intergranular corrosion and intergranular stress corrosion cracking often occur, causing huge economic losses to enterprises and seriously endangering production and personal safety. Therefore, how to improve the intergranular corrosion resistance and intergranular stress corrosion resistance of austenitic stainless steel is of great significance to prolong the service life of stainles...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): C21D1/18C21D8/02C21D8/06C21D1/26
CPCC21D1/18C21D1/26C21D8/0221C21D8/0247C21D8/065C21D2211/001
Inventor 冯文雷晓陈劲松杨建明丁云飞
Owner HUAIHAI INST OF TECH