Slurry mixing method for silicon-carbon negative electrode
A negative electrode slurry, silicon carbon technology, applied in the direction of negative electrode, battery electrode, active material electrode, etc., can solve the problems of easy to cause climbing rod effect, low solid content of slurry, high powder viscosity, etc., to avoid damage and Climbing pole phenomenon, solving the effect of low solid content and good dispersion
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Embodiment 1
[0028] The concrete steps of the method for mixing the slurry of the silicon-carbon negative electrode in this embodiment are as follows:
[0029] S1. Stir 1 kg of polyacrylic acid binder with a mass fraction of 12.8% and 1.3 kg of water under vacuum conditions for 100 min to obtain glue A. The stirring parameters are 30 rpm for rotation and 30 rpm for revolution;
[0030] S2. Add 0.5 kg of liquid conductive agent CNT with a solid content of 0.4% to glue A and stir for 240 minutes to obtain glue B. The stirring parameters are 1000 rpm for rotation and 1000 rpm for revolution;
[0031] S3. Add 2kg negative electrode powder SiOx / C-600A, 0.04kgSP, 0.02kgKS-6 and 0.3kg water to the glue B, first stir at low speed for 10min (rotation 30rpm, revolution 30rpm), then high-speed stirring (rotation 1000rpm, After revolution (1000rpm) for 240min, add water and rotate at 20rpm for 30min under vacuum to defoam and adjust viscosity to obtain silicon carbon negative electrode slurry.
Embodiment 2
[0033] The concrete steps of the method for mixing the slurry of the silicon-carbon negative electrode in this embodiment are as follows:
[0034] S1. Stir 1kg of polyacrylic acid binder with a mass fraction of 12.8%, 0.4kg of liquid conductive agent CNT with a solid content of 0.5%, and 1.3kg of water under vacuum conditions for 240min to obtain glue B. The stirring parameter is 40rpm , revolution 40rpm;
[0035] S2. Add 2kg of negative electrode powder SiOx / C-600A, 0.04kg of SP, 0.02kg of KS-6 and 0.3kg of water to the glue B, first stir at low speed for 10min (rotation 30rpm, revolution 30rpm), then stir at high speed (rotation 1200rpm, After revolution (1200rpm) for 240min, add water and rotate at 25rpm for 30min under vacuum to defoam and adjust viscosity to obtain silicon carbon negative electrode slurry.
Embodiment 3
[0037] S1. Stir 0.85kg of styrene-butadiene rubber (SBR) / carboxymethyl cellulose sodium (CMC) binder with a mass fraction of 12.8% and water for 0.5h under vacuum to obtain a solid content of 5% to 8%. Glue A, the stirring parameters are rotation 10rpm, revolution 10rpm;
[0038] S2. Add 1.08 kg of liquid conductive agent CNT with a solid content of 0.2% to the glue A and stir for 3 hours to obtain the glue B. The stirring parameters are 400 rpm for rotation and 400 rpm for revolution;
[0039] S3. Add 2kg negative electrode powder SiOx / C-600A, 0.03kgSP, 0.02kgKS-6 and water to the glue B, first stir at low speed (rotation 100rpm, revolution 100rpm) for 0.1h, then stir at high speed (rotation 400rpm, revolution 400rpm) 5h, then add water and rotate at 30rpm under vacuum for 0.15h to defoam and adjust viscosity to obtain a silicon-carbon negative electrode slurry with a solid content of 35%~45%.
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