Nickel-based powder superalloy and its preparation method and application
A technology of superalloy and nickel-based powder, applied in the field of powder superalloy, can solve the problem of inability to meet long-lasting high performance, achieve uniform microstructure, uniform alloy composition, and improve the degree of alloying
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Embodiment 1
[0061] The preparation of embodiment 1 nickel base powder superalloy
[0062] Prepare 1 with the ingredients listed in Table 1 and their contents as raw materials # ~5 # Nickel based powder superalloy.
[0063] Table 1 Composition and preparation conditions of nickel-based powder superalloy samples
[0064]
[0065]
[0066] The preparation method is as follows:
[0067] S1. Prepare raw materials according to the chemical composition and mass fraction of the powdered superalloy, and prepare alloy rods by using a 25kg vacuum induction melting process;
[0068] S2. Using the plasma rotating electrode method to prepare superalloy powder from the alloy bar, the alloy powder is screened and electrostatically treated to obtain a finished powder with a particle size of 50 μm to 150 μm;
[0069] S3. The alloy powder is put into a low-carbon steel ladle for vacuum degassing and sealing welding;
[0070] S4. Perform hot isostatic pressing to the alloy powder after sealing and...
experiment example 1
[0072] Experimental example 1 Metallographic structure characterization of nickel-based powder superalloy
[0073] Adopt Olympus GM-7 type metallographic microscope to observe the microstructure of alloy after heat treatment state and long-term aging, characterize the 1 prepared in embodiment 1 # ~5 # Metallographic structure of nickel-based powder superalloys.
[0074] to 4 # Nickel-based powder superalloy is typical, and its metallographic structure in the heat treatment state is as follows: figure 1 shown; 4 # The metallographic structures of nickel-based powder superalloy after aging at 815℃ / 3000h and after aging at 850℃ / 500h are as follows: figure 2 and image 3 shown.
[0075] The microstructure of the nickel-based powder superalloy provided by the present invention is mainly composed of γ, γ′, MC and M3B2 phases, and the composition of the γ′ phase is (Ni, Co) 3 (Al, Ti, Ta, Nb, Hf) type, the composition of MC type carbide is (Ti, Ta, Nb, Hf) C type.
[0076] 1...
experiment example 2
[0081] Performance Characterization of Experimental Example 2 Nickel-based Powder Superalloy
[0082] Adopt NCS GNT100 electronic tensile testing machine, GNCJ-30 mechanical type high temperature durable creep testing machine to test the 1 prepared in embodiment 1 # ~5 # Mechanical properties of nickel-based powder superalloys.
[0083] Among them, 1 # ~5 # The room temperature tensile properties, 760°C tensile properties, 815°C tensile properties, and 815°C / 450MPa durability properties of nickel-based powder superalloys are listed in Table 2, Table 3, Table 4, and Table 5, respectively.
[0084] Table 2 Room temperature tensile properties of nickel-based powder superalloys
[0085] Alloy No. σ b / MPa
σ 0.2 / MPa
δ / % ψ / % 1 #
1570 1210 11.0 12.5 2 #
1605 1240 10.0 11.5 3 #
1565 1205 11.5 12.5 4 #
1583 1225 11.0 12.0 5 #
1620 1260 9.0 10.5
[0086] Table 3 Tensile properties of nickel-based ...
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