Using method of aromatic hydrocarbon enriched wax oil in heavy oil up-flowing type hydrogenation thermal cracking reaction process
A technology of cracking reaction and hydrogenation reaction, which is applied in the direction of only multi-stage series refining and cracking process, treatment of hydrocarbon oil, petroleum industry, etc., and can solve the problems of lower overall economy, long hydrogenation process, and no reports. , to achieve the effect of saving system scale, reducing hydrogen consumption and improving economy
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[0759] Example one
[0760] Based on the comparative example, in order to increase the overall conversion rate of the hydrothermal cracking feedstock oil vacuum residue, the use of the aromatic-rich wax oil of the present invention in the heavy oil upflow hydrothermal cracking reaction process is used, and the steps are as follows:
[0761] The wax oil catalytically cracked heavy cycle oil (catalytically cracked wax oil) is used as aromatic-rich wax oil (aromatic-rich intermediate wax oil) and added to the second reactor of the suspended bed hydrothermal cracking reaction R10 of vacuum residue R10F Without passing through the first reactor R10A, the ratio of the weight of aromatic-rich medium wax oil to the weight of vacuum residue R10F is 20%;
[0762] Under the condition that the yield of benzene insolubles in the oil produced by the hydrothermal cracking reaction of vacuum residue R10F does not increase (not more than 2.2 to the mass% of the feed oil), the single-pass conversion r...
Example Embodiment
[0763] Example two
[0764] Based on Example 1, in order to improve the overall hydrothermal cracking conversion rate of vacuum residue R10F, the present invention is used to perform cyclic hydrothermal cracking of the hydrothermal cracked product heavy wax oil and residual oil.
[0765] In the hydrothermal cracking product fractionation step, vacuum fractionation deep draws the hydrothermal cracking medium wax oil THC-KVGO, and the suspended bed hydrothermal cracking product residue oil (>475℃) is separated into three fractions:
[0766] The first fraction is the medium wax oil THC-MVGO (mainly composed of hydrocarbons with a conventional boiling point of 400-520°C) as the R10 product of the heavy oil hydrothermal cracking reaction process;
[0767] The second fraction is THC-HVGO, a heavy oil of the hydrothermal cracking product, which is mainly composed of hydrocarbons with a conventional boiling point of 510 to 550°C, which is the feed and washing section of the R10 product vacuum ...
Example Embodiment
[0777] Example three
[0778] Based on the second embodiment, the recycling method of light hydrogen supply solvent is adopted to ease the operating conditions of the front reaction section R10A of the vacuum residue hydrothermal cracking reaction process R10 (mainly reducing the operating temperature), and further improve the hydrothermal cracking The overall thermal cracking conversion rate of the raw oil vacuum residue R10F reduces the number of external residues.
[0779] In order to alleviate the operating conditions of R10A in the front reaction section of the vacuum residue hydrothermal cracking reaction process R10 (mainly to reduce the operating temperature), and to further increase the overall thermal cracking conversion rate of the hydrothermal cracking feedstock oil vacuum residue R10F , Under the premise of fully improving the hydrogen supply efficiency of the external light hydrogen supply solvent DS and the hydrogen transfer efficiency in the reactor of the front hyd...
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