Preparation method of carboxylated acrylonitrile butadiene rubber latex with high solid content

A technology of carboxylated nitrile latex and high solid content, which is applied in the field of preparation of high solid content carboxylated nitrile latex, can solve the problems of complex preparation methods of carboxylated top tight latex, unfavorable stable and efficient production, unsatisfactory use effect, etc., to achieve improvement Alkali resistance and anti-oxidation effect, beneficial to the promotion of use, and the effect of improving quality and performance

Inactive Publication Date: 2019-12-31
DONGYING JIUZHOU AOHUA CHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] However, the existing method of preparing carboxy-top tight latex is relatively complicated, which is not conducive to stable and efficient production, and the material configuration in the existing method is unreasonable, the solid content of the latex is low, and the use effect is not ideal, so it needs to be improved for production

Method used

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Examples

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Effect test

preparation example Construction

[0028] A preparation method of carboxylated nitrile latex with high solid content, the preparation method of the high solid content carboxylated nitrile latex is made of the following raw materials: carboxylated nitrile rubber 20%-30%, phenolic rubber 15%-25%, ethylene glycol Ethylene glycolate 10%-20%, dimethyl sebaceous acid 5%-15%, silicone waterproofing agent 5%-10%, modified starch 15%-25% and deionized water 5%-15%.

[0029] As preferably, described comprises the steps:

[0030] S1. Weigh each raw material according to the mass percentage, and set aside;

[0031] S2. Put carboxylated nitrile rubber, phenolic rubber, ethylene glycol oxalate and dimethyl sebumate into the mixer, and stir evenly for 15 minutes to 20 minutes at a rate of 20 rpm to 30 rpm. get the mixed material,

[0032] S3, adding deionized water to the mixed material, heating to 70°C to 80°C, and keeping it warm for 2 hours to 3 hours to obtain a latex;

[0033] S4, adding a silicone water repellent to ...

Embodiment 1

[0050] A preparation method of carboxylated nitrile latex with high solid content, the preparation method of the high solid content carboxylated nitrile latex is made of the following raw materials: 25% carboxylated nitrile rubber, 20% phenolic rubber, 10% ethylene glycol oxalate , Dimethyl Sebaceate 15%, Silicone Water Repellent 5%, Modified Starch 20% and Deionized Water 5%.

[0051] As preferably, described comprises the steps:

[0052] S1. Weigh each raw material according to the mass percentage, and set aside;

[0053] S2. Put carboxylated nitrile rubber, phenolic rubber, ethylene glycol oxalate and dimethyl sebumate into the mixer, and stir evenly for 15 minutes to 20 minutes at a rate of 20 rpm to 30 rpm. get the mixed material,

[0054] S3, adding deionized water to the mixed material, heating to 70°C to 80°C, and keeping it warm for 2 hours to 3 hours to obtain a latex;

[0055] S4, adding a silicone water repellent to the latex, and stirring evenly for 3 to 5 minu...

Embodiment 2

[0071] A preparation method of carboxylated nitrile latex with high solid content, the preparation method of the high solid content carboxylated nitrile latex is made of the following raw materials: 20% carboxylated nitrile rubber, 20% phenolic rubber, 15% ethylene glycol oxalate , Dimethyl Sebaceate 15%, Silicone Water Repellent 5%, Modified Starch 20% and Deionized Water 5%.

[0072] As preferably, described comprises the steps:

[0073] S1. Weigh each raw material according to the mass percentage, and set aside;

[0074] S2. Put carboxylated nitrile rubber, phenolic rubber, ethylene glycol oxalate and dimethyl sebumate into the mixer, and stir evenly for 15 minutes to 20 minutes at a rate of 20 rpm to 30 rpm. get the mixed material,

[0075] S3, adding deionized water to the mixed material, heating to 70°C to 80°C, and keeping it warm for 2 hours to 3 hours to obtain a latex;

[0076] S4, adding a silicone water repellent to the latex, and stirring evenly for 3 to 5 minu...

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PUM

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Abstract

The invention discloses a preparation method of carboxylated acrylonitrile butadiene rubber latex with high solid content. The preparation method of the carboxylated acrylonitrile butadiene rubber latex with high solid content comprises that the carboxylated acrylonitrile butadiene rubber latex is prepared from the following raw materials: 20%-30% of carboxylated butadiene-acrylonitrile rubber, 15%-25% of phenolic rubber, 10%-20% of ethanedioic acid diethyl ester, 5%-15% of dimethyl sebacate, 5%-10% of an organosilicone waterproof agent, 15%-25% of modified starch and 5%-15% of deionized water. According to the preparation method of the carboxylated acrylonitrile butadiene rubber latex with high solid content, production and processing are carried out by adopting a reasonable material ratio; the technological process is simple and easy to control, and efficient production is facilitated; meanwhile, the solid content is improved by adding the modified starch, the quality and performanceof the latex are effectively improved, improvement of the alkali-resistant and antioxidant effects is facilitated, and application and popularization are facilitated.

Description

technical field [0001] The invention relates to the technical field of nitrile latex, in particular to a method for preparing carboxylated nitrile latex with high solid content. Background technique [0002] In the current industrial production, carboxylated nitrile latex is widely used, so large-scale and efficient production is required. [0003] However, the existing method of preparing carboxy-topped latex is relatively complicated, which is not conducive to stable and efficient production. In addition, the material configuration in the existing method is unreasonable, the solid content of the latex is low, and the use effect is not ideal, so it needs to be improved for production. Contents of the invention [0004] The objective of the invention is in order to solve the shortcoming that exists in the prior art, and the preparation method of a kind of high solid content carboxylated nitrile latex that proposes. [0005] In order to achieve the above object, the presen...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L13/02C08L61/06C08L3/10C08K5/11C08B31/18C08B31/04
CPCC08B31/04C08B31/185C08L13/02C08L2201/08C08L2205/03C08L61/06C08L3/10C08K5/11
Inventor 王旭
Owner DONGYING JIUZHOU AOHUA CHEM
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