A kind of manufacturing process of polyphenylene sulfide film
A technology of polyphenylene sulfide film and manufacturing process, which is applied in the field of polyphenylene sulfide film manufacturing process, and can solve problems such as complex film production process and process conditions
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Embodiment 1
[0046] First, sodium hydrosulfide and sodium hydroxide are added to N-methyl-2-pyrrolidone solvent, and then oxygen-free deionized water of 9 mol / mol NaHS is added to make NaHS in the system: NaOH: NMP: H 2 The molar ratio of O is 1.0:1.16:1.5:10.0; heated to 148°C at a heating rate of 2.0°C / min, kept at this temperature for 1.5h, and then heated to 183°C at a heating rate of 1.0°C / min. Insulate for 1.5 hours, then raise the temperature to 213°C. Under this temperature condition, keep hold for 8 minutes, and then drop the temperature to 203°C. After the system materials are processed by such a treatment process, the Na in the system 2 S:NMP:H 2 The mol ratio of O is 1.0: 0.6: 1.1; Add p-dichlorobenzene, hexachlorobenzene raw material and NMP solvent again, make the Na of the system 2 S:p-DCB:Hexachlorobenzene:NMP:H 2 The molar ratio of O is 1.0: 0.98: 0.13: 3.3: 1.1; then the temperature of the system is raised to 218°C. Under this temperature condition, after 4.5h of heat p...
Embodiment 2
[0051] First, sodium hydrosulfide and sodium hydroxide are added to the N-methyl-2-pyrrolidone solvent, and then 11mol / mol NaHS oxygen-free deionized water is added to make the NaHS in the system: NaOH: NMP: H 2 The molar ratio of O is 1.0:1.19:1.8:12.0; heated to 158°C at a heating rate of 3.0°C / min, kept at this temperature for 1.0h, and then heated to 188°C at a heating rate of 2.0°C / min. Keep warm for 1.0h, and then raise the temperature to 233°C. Under this temperature condition, keep warm for 3 minutes, and then drop the temperature to 206°C. After the system materials are processed by such a treatment process, the Na in the system 2 S:NMP:H 2 The mol ratio of O is 1.0: 0.9: 1.8; Add p-dichlorobenzene, hexachlorobenzene raw material and NMP solvent again, make the Na of system 2 S:p-DCB:Hexachlorobenzene:NMP:H 2 The molar ratio of O is 1.0:0.99:0.18:3.3~3.8:1.8; then the temperature of the system is raised to 222°C. Under this temperature condition, after 3.0 hours of ...
Embodiment 3
[0061] First, sodium hydrosulfide and sodium hydroxide are added to the N-methyl-2-pyrrolidone solvent, and then 10mol / mol NaHS oxygen-free deionized water is added to make the NaHS in the system: NaOH: NMP: H 2 The molar ratio of O is 1.0:1.17:1.6:11.0; heated to 151°C at a heating rate of 2.3°C / min, kept at this temperature for 1.2h, and then heated to 184°C at a heating rate of 1.3°C / min. Insulate for 1.4 hours, then raise the temperature to 225°C. Under this temperature condition, keep hold for 6 minutes, and then drop the temperature to 204°C. After the system materials are processed by such a treatment process, the Na in the system 2 S:NMP:H 2 The mol ratio of O is 1.0: 0.7: 1.4; Add p-dichlorobenzene, hexachlorobenzene raw material and NMP solvent again, make the Na of the system 2 S:p-DCB:Hexachlorobenzene:NMP:H 2 The molar ratio of O is 1.0: 0.983: 0.143: 3.5: 1.4; then the temperature of the system is raised to 220°C. Under this temperature condition, after 3.5 hou...
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