A kind of tunnel water-based high-brightness and easy-to-clean porcelain paint and preparation method thereof
An easy-to-clean, water-based technology, applied in anti-corrosion coatings, reflective/signal coatings, polyurea/polyurethane coatings, etc., can solve the problems of difficult degradation and diffusion of harmful substances, general luminous effect, poor reflective effect, etc., and achieve good compactness , The surface is smooth and smooth, and the effect is easy to control
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[0032] A preparation method of a tunnel water-based highlighting and easy-cleaning vitrified coating is as follows:
[0033] Firstly, the hydrophobic modified reflective micro-beads are prepared, and the specific preparation process is as follows:
[0034] Hydrophobic modified reflective beads are prepared by the following process:
[0035](1) According to mass percentage, after mixing 12-15% of lithium chloride, 14-40% of titanium chloride, 16-30% of aluminum nitrate and 16-25% of lanthanum nitrate, add it to 12-15% of water and mix and stirring at a stirring rate of 300 rpm, heated in a water bath to 50°C, then dropwise added 0.1-1% sodium hydroxide solution with a mass concentration of 20%, filtered after stirring for 3 hours, washed the filter cake and dispersed it in water, Heating in a water bath at 50°C and stirring, adding acetic acid dropwise to pH=4-5, and stirring for 3 hours to obtain the first sol;
[0036] (2) According to the mass percentage, add 30-43% of eth...
Embodiment 1
[0047] The preparation method of the water-based high-brightness and easy-to-clean porcelain coating for tunnels is as follows:
[0048] (1) In terms of mass percentage, after mixing 12% of lithium chloride, 40% of titanium chloride, 16% of aluminum nitrate and 19.9% of lanthanum nitrate, they are added to 12% of water, mixed and stirred, and the stirring rate is 300 rpm / per minute, heated to 50°C in a water bath, then added dropwise 0.1% sodium hydroxide solution with a mass concentration of 20%, filtered after stirring for 3 hours, washed the filter cake and dispersed it in water, heated in a water bath to 50°C with stirring, and added dropwise acetic acid to pH= 4-5, stirring for 3 hours to obtain the first sol;
[0049] (2) In terms of mass percentage, 30% ethyl orthosilicate and 30% methyl triethoxysilane were added to dissolve in 25% ethanol, and 15% water was added under stirring, then acetic acid was added to adjust the pH value to 4-5, and then The first sol was ad...
Embodiment 2
[0059] In Example 2, the weight ratio of composition A to curing agent is 100:20, and the components of composition A are shown in Table 2.
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