Hydrogenolysis catalyst structure, hydrogenolysis device provided with said hydrogenolysis catalyst structure, and production method of hydrogenolysis catalyst structure
A technology for hydrocracking and a manufacturing method is applied in the manufacture of a catalyst structure for hydrocracking and the field of hydrocracking devices, which can solve the problems of expensive equipment and large amount of process energy, and achieve high-efficiency hydrocracking treatment. , the effect of reducing the catalytic activity
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Embodiment 1～384
[0120] [Synthesis of precursor material (A)]
[0121] A mixed aqueous solution obtained by mixing a silica agent (tetraethoxysilane (TEOS), manufactured by Wako Pure Chemical Industries, Ltd.) and a surfactant as a templating agent was prepared, and the pH was adjusted appropriately. The hydrothermal treatment was carried out under the treatment conditions of ~350°C and 100 hours. Then, the generated precipitate was filtered, washed with water and ethanol, and fired at 600° C. in air for 24 hours to obtain precursor materials (A) of the types and pore sizes shown in Tables 1 to 8. In addition, as surfactant, the following thing was used according to the kind of precursor material (A) ("kind of precursor material (A): surfactant").
[0122] ・MCM-41: cetyltrimethylammonium bromide (CTAB) (manufactured by Wako Pure Chemical Industries, Ltd.)
[0123] · SBA-1: Pluronic P123 (manufactured by BASF Corporation)
[0124] [Production of precursor materials (B) and (C)]
[0125] Nex...
Embodiment 385～768
[0141] In Examples 385 to 768, except that the conditions in the synthesis of the precursor material (A) and the preparation of the precursor materials (B) and (C) were changed as in Tables 9 to 16, the same procedure as in Example 1 was carried out. The method yields precursor material (C). In addition, the following metal salts were used depending on the type of metal microparticles|fine-particles ("metal microparticles|metal salts") used when preparing the metal-containing aqueous solution.
[0142] Co: cobalt(II) nitrate hexahydrate (manufactured by Wako Pure Chemical Industries, Ltd.)
[0143] Ni: nickel(II) nitrate hexahydrate (manufactured by Wako Pure Chemical Industries, Ltd.)
[0144] ・Fe: iron(III) nitrate nonahydrate (manufactured by Wako Pure Chemical Industries, Ltd.)
[0145] Cu: Copper(II) nitrate trihydrate (manufactured by Wako Pure Chemical Industries, Ltd.)
[0146] [Synthesis of Catalyst Structure]
[0147] Mix the precursor material (C) obtained above...
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