Siloxane organic fluorescent powder and preparation method thereof
A siloxane and phosphor technology, applied in luminescent materials, chemical instruments and methods, sustainable buildings, etc., can solve problems such as inability to apply, characteristics cannot meet requirements, etc., to improve optoelectronic characteristics, improve reliability, and improve dispersion. sexual effect
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example 1
[0050] In this example, the organic dye is selected from C545T, such as figure 2 Siloxane (Siloxane), such as figure 1 method to make organic phosphors. Figure 5 The PL excitation spectrum (left) and PL emission spectrum (right) of the siloxane organic phosphor prepared in Example 1 are shown, and the excitation spectrum is the absorption spectrum. At the same time, the PL excitation spectrum (left) and PL emission spectrum (right) of the simple organic dye C545T are also placed for comparison. Such as Figure 5 As shown, the optimum excitation range of the siloxane organic phosphor powder prepared in Example 1 falls within 440-470nm (the emission range of commercial blue light LEDs), and the emitted light wavelength falls within 500-530nm. The conversion efficiency of the green light-emitting siloxane organic phosphor is higher than 95%, and its luminous efficiency is better than that of the organic dye C545T.
example 2
[0052] In this example, DCJTB is selected as the organic dye, using such as figure 2 Siloxane (Siloxane), such as figure 1 The method is made of siloxane organic phosphor. Image 6 The PL excitation spectrum (left) and PL emission spectrum (right) of the siloxane organic phosphor prepared in Example 2 are shown. At the same time, the PL excitation spectrum (left) and PL emission spectrum (right) of the simple organic dye DCJTB are also placed for comparison. Such as Image 6 As shown, the optimum excitation range of the siloxane organic phosphor powder prepared in Example 2 falls within 440-470nm (the emission range of commercial blue light LEDs), and the emitted light wavelength falls within 600-630nm. The conversion efficiency of the red light-emitting siloxane organic phosphor is higher than 90%, and the luminous efficiency is better than that of the organic dye DCJTB.
example 3
[0054] In this example, the organic dye is selected from TPA, such as figure 2 Siloxane (Siloxane), such as figure 1 The method is made of siloxane organic phosphor. Figure 7 The PL excitation spectrum (left) and PL emission spectrum (right) of the siloxane organic phosphor prepared in Example 3 are shown. At the same time, put the PL excitation spectrum (left) and PL emission spectrum (right) of the pure organic dye TPA for comparison. Such as Figure 7 As shown, the optimum excitation range of the siloxane organic phosphor powder prepared in Example 3 falls within 440-470nm (the emission range of commercial blue LEDs), and the emission wavelength falls within 500-530nm. The conversion efficiency of the green light-emitting siloxane organic phosphor is higher than 90%, and the luminous efficiency is better than that of the organic dye TPA.
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