Composite solid electrolyte and all-solid-state battery
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Embodiment 1
[0163] [Production of composite solid electrolyte]
[0164] All experimental operations were carried out in a glove box controlled by Ar gas with a dew point below -70°C.
[0165] As the first sulfide-based solid electrolyte particles, Li 6 P.S. 5 Cl crystal particles.
[0166] The first sulfide-based solid electrolyte particles had an average particle diameter (D50) of 0.5 μm, a Young's modulus of 80 GPa, an aspect ratio of 2, a major axis length of the particles of 1 μm, and a lithium ion conductivity of 1 mS / cm.
[0167] As the second sulfide-based solid electrolyte particles, LiI-LiBr-Li was prepared 3 P.S. 4 Glass ceramic particles.
[0168] The second sulfide-based solid electrolyte particles had an average particle diameter (D50) of 3 μm, a Young's modulus of 15 GPa, an aspect ratio of 1, a major axis length of the particles of 3 μm, and a lithium ion conductivity of 3.2 mS / cm.
[0169] Put the first sulfide-based solid electrolyte particles and the second sulfide...
Embodiment 2
[0171] Put the first sulfide-based solid electrolyte particles and the second sulfide-based solid electrolyte particles into the mortar so that the first sulfide-based solid electrolyte particles: the second sulfide-based solid electrolyte particles = 1:99 (mass % ) except for the mixing ratio, a composite solid electrolyte was produced in the same manner as in Example 1.
Embodiment 3
[0173] Put the first sulfide-based solid electrolyte particles and the second sulfide-based solid electrolyte particles into the mortar so that the first sulfide-based solid electrolyte particles: the second sulfide-based solid electrolyte particles = 5: 95 (mass % ) except for the mixing ratio, a composite solid electrolyte was produced in the same manner as in Example 1.
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