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Method and application of polyvinyl alcohol fiber composite material prepared by step-by-step hot rolling modification

A polyvinyl alcohol fiber and composite material technology, applied in the direction of improved hand feeling fiber, fiber treatment, fiber type, etc., can solve the problems such as the inability to directly obtain modified polyvinyl alcohol fiber composite materials, and achieve improved mechanical properties, fracture elongation, etc. Increased elongation and firm fiber knots

Active Publication Date: 2021-12-21
SOUTH CHINA UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the above methods all require secondary processing, and it is impossible to directly obtain a modified polyvinyl alcohol fiber composite material with thermoplastic and heat-sealing properties.

Method used

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  • Method and application of polyvinyl alcohol fiber composite material prepared by step-by-step hot rolling modification
  • Method and application of polyvinyl alcohol fiber composite material prepared by step-by-step hot rolling modification
  • Method and application of polyvinyl alcohol fiber composite material prepared by step-by-step hot rolling modification

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0049] It is used for the preparation of step-by-step hot rolling modified non-woven fabrics, including the following steps:

[0050] ①Preparation of sizing modified solution (agent) for step-by-step hot-rolled modified non-woven fabrics:

[0051] In parts by weight, it includes the following components:

[0052]

[0053] After the above-mentioned components are measured separately, they are respectively added into the dissolution container with a stirring and heating device, and the stirring is started at a stirring rate of 80 rpm, and the heating is started, and the temperature is raised to a temperature range of 95°C. Keep it under high temperature for 2 hours to ensure that the polyvinyl alcohol is completely dissolved, lower the temperature to 90° C. and keep it warm for 1 hour for homogenization treatment, then cool to room temperature and discharge for later use to obtain a polyvinyl alcohol non-woven fabric sizing modification solution (agent).

[0054] ②Use the gl...

Embodiment 2

[0063] It is used for the preparation of step-by-step hot rolling modified non-woven fabrics, including the following steps:

[0064] ①Preparation of sizing modified solution (agent) for step-by-step hot-rolled modified non-woven fabrics:

[0065] In parts by weight, it includes the following components:

[0066]

[0067] After the above-mentioned components are measured separately, add them into the dissolution container with a stirring and heating device, start stirring at a stirring rate of 250 rpm, and start heating to a temperature range of 100°C. Keep it under high temperature for 4 hours to ensure that the polyvinyl alcohol is completely dissolved, lower the temperature to 90° C. and keep it warm for 0.5 hour for homogenization treatment, then cool to room temperature and discharge for later use to obtain a polyvinyl alcohol non-woven fabric sizing modification solution (agent).

[0068] ②Use the gluing modification solution (agent) prepared in step ① to prepare polyv...

Embodiment 3

[0077] It is used for the preparation of step-by-step hot rolling modified non-woven fabrics, including the following steps:

[0078] ①Preparation of sizing modified solution (agent) for step-by-step hot-rolled modified non-woven fabrics:

[0079] In parts by weight, it includes the following components:

[0080]

[0081] After the above-mentioned components are measured separately, they are respectively added into a dissolution container with a stirring and heating device, and the stirring is started at a stirring rate of 150 rpm, and heating is started to raise the temperature to a temperature range of 98°C. Keep it under high temperature for 3 hours to ensure that the polyvinyl alcohol is completely dissolved, cool down to 90° C. and keep warm for 0.6 hours for homogenization treatment, then cool to room temperature and discharge for later use to obtain a polyvinyl alcohol non-woven fabric sizing modification solution (agent).

[0082] ②Use the gluing modification solut...

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Abstract

The invention discloses a method and application of a polyvinyl alcohol fiber composite material prepared by a step-by-step hot rolling modification method. The method comprises: using modified glue solution (agent) and polyvinyl alcohol fiber produced by wet spinning in the non-woven fabric preparation process to carry out step-by-step gluing, hot-rolling, modification and compounding. Glue modifying solution (agent), by parts by weight, includes the following components: polyvinyl alcohol 100; modified polyol plasticizer 20‑100; softener 5‑10; filler 3‑10; wetting penetrating agent 0.2‑1.0; antifungal agent 0.3‑1.0; water 400‑600. The non-woven fabric prepared by the above process can greatly improve its heat sealing performance and strengthen mechanical and physical properties, and its hand feeling is also improved.

Description

technical field [0001] The invention relates to the field of fiber composite material preparation, in particular to a method and application for preparing polyvinyl alcohol fiber composite material by a step-by-step hot rolling modification method. Background technique [0002] As an environmentally friendly material, polyvinyl alcohol (PVA) has been rapidly developed and applied in many fields in recent years. Polyvinyl alcohol (PVA) materials have abundant sources of raw materials and relatively mature production processes, especially in the field of fiber production and application, the mature production process of vinylon fibers produced with polyvinyl alcohol as the main raw material is wet The method of spinning is the aqueous solution spinning method, and the preparation of polyvinyl alcohol non-woven fabrics is in the pre-production process of vinylon, polyvinyl alcohol (PVA) is formed by the wet spinning coagulation bath of polyvinyl alcohol fibers, not to continue ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D04H1/4309D04H1/64D04H1/54D04H1/587D06M15/333D06M13/419D06M15/53D06M11/79D06M13/188D06M13/203D06M101/24
CPCD04H1/4309D04H1/64D04H1/54D04H1/587D06M15/333D06M13/419D06M15/53D06M11/79D06M13/188D06M13/203D06M2101/24D06M2200/50
Inventor 崔跃飞崔若曦
Owner SOUTH CHINA UNIV OF TECH