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697results about How to "Low requirements for production equipment" patented technology

Fe-based nanocrystalline soft magnetic alloy with strong amorphous forming ability and preparing method of Fe-based nanocrystalline soft magnetic alloy

The invention discloses a Fe-based nanocrystalline soft magnetic alloy with strong amorphous forming ability and a preparing method of the Fe-based nanocrystalline soft magnetic alloy. The alloy has an expression of Fe<x>SiBP<c>Nb<d>Cu<e>, wherein in the expression, each of the x, the a, the b, the c, the d and the e shows the atomic percentage content of the corresponding ingredient, and meets the following conditions that the a is greater than or equal to 0.5 but smaller than or equal to 12; the b is greater than or equal to 0.5 but is smaller than or equal to 15; the c is greater than or equal to 0.5 but smaller than or equal to 12; the d is greater than or equal to 0.1 but smaller than or equal to 3; the e is greater than or equal to 0.1 but smaller than or equal to 3; the x is greater than or equal 70 but smaller than or equal to 85; and the sum of the x, the a, the b, the c, the d and the e is 100 percent. The soft magnetic alloy has the advantages that an ordinary copper mold casting method can be used for preparing a Fe-based amorphous alloy with the critical dimension being 3.5mm; after the annealing; the saturation flux density is greater than 1.5T; and the coercive force value is smaller than 1A/m.
Owner:ADVANCED TECHNOLOGY & MATERIALS CO LTD

Vinegar koji and biological edible vinegar, and method of producing the same

The invention relates to a vinegar melody, biological vinegar and the preparing method, which dissolve the problem that glacial acetic acid or the like in the edible vinegar has side effect for the human. The vinegar melody is made by Avena sativa, wheat, black rice, peart barley, soya bean, black soya bean, green bean, red bean, broad bean, pea, tea, traditional Chinese medicine herbal pieces prepared for decoction and vinegar melody bacterial. The preparing method of the vinegar melody comprises the following steps: 1, boiling after disintegrating high starch raw material and infiltrating with the water; 2, adding the other raw material, water and vinegar melody bacterial and fermenting. The biological vinegar is made by vinegar melody, Daqu, Shenqu, bran melody, wine yeast, aspergillus oryzae, Chinese sorghum, corn, millet, glutinous millet, peart barley, glutinous rice, black rice, citrate bacterial, yeast, acetic acid bacteria and fruit normal juice. The preparing method of the biological vinegar comprises the following steps: 1, boiling after disintegrating high starch raw material and infiltrating with the water; 2, adding the other raw material and saccharifying and acetous fermenting zymogeneous bacteria; 3, adding the salt and afterripening; 4, drenching the vinegar; ageing; sterilizing and filtering. The local flavor of the biological vinegar comes from the raw material and the metabolite of the microorganism completely without the glacial acetic acid or the like, and the biological vinegar doesn't have the side effect for the human and has the delicious taste and more than 8. 13g / 100ml high vinegar yield.
Owner:范英祝

Preparation method of graphene coating polyacrylonitrile fiber composite material

The invention relates to a preparation method of a graphene coating polyacrylonitrile fiber composite material. The preparation method comprises the following steps of: (1) processing polyacrylonitrile by using alkali; (2) preparing a polyacrylonitrile fiber with modified single layer KH550; (3) preparing a polyacrylonitrile fiber with modified single layer graphite oxide; (4) using the polyacrylonitrile fiber with the modified single layer graphite oxide as a raw material, repeating the step (2) and the step (3), and obtaining the polyacrylonitrile fiber with modified multiplayer graphite oxide; and (5) placing the polyacrylonitrile fiber with the modified multiplayer graphite oxide in a graphite oxide dispersion liquid, then dropwise adding a hydrazine hydrate aqueous solution, carrying out heating reaction, finally cooling, washing and drying to obtain the graphene coating polyacrylonitrile fiber composite material. The preparation method provided by the invention is simple; the graphite of the composite material provided by the invention is good in reduction degree and uniformly coats the surface of the polyacrylonitrile; and compared with a commercial finished product, the composite material has the advantages that the resistivity of a single wire is reduced by six order of magnitudes, and the composite material has the application prospect of conductive fiber preparation.
Owner:SHENGQUAN HEALTANG

Formula and film-coating preparation method for biological carbon coated urea

The invention relates to a formula and a film-coating preparation method for biological carbon coated urea. The biological carbon coated urea is characterized in that the outside of a fertilizer core is coated with solid-powder-shaped biological carbon, sulfur, dicyandiamide and bentonite by using granular urea with a size of 3 to 4 mm as the fertilizer core and oxidized corn starch as bonding liquid, wherein the above-mentioned components have weight proportions as follows: 50 to 80 parts of the urea, 10 to 30 parts of the biological carbon, 2 to 10 parts of the sulfur, 2 to 3 parts of the dicyandiamide, 2 to 3 parts of the bentonite and 3 to 5 parts of the corn starch. The film-coating preparation method for the biological carbon coated urea comprises the following steps: placing the urea into a disc granulator, carrying out preheating with hot air for 5 min, spraying the bonding liquid on the surface of the urea with a high-pressure spray gun, blowing the hot air for 3 to 5 min, adding a mixed film-coating material into the disc granulator in batches and carrying out rotating for 10 min, then spraying the bonding liquid again, and carrying out drying in the air so as to obtain the biological carbon coated urea. According to the invention, the biological carbon can improve physical and chemical properties of soil and adsorb ammonium-nitrogen and nitrate-nitrogen ions; the dicyandiamide reduces nitrification; and S4O62- generated by decomposition of the sulfur can delay decomposition of the dicyandiamide, and H+ and S2O32- generated by decomposition of the sulfur can inhibit nitrification. The biological carbon coated urea provided by the invention has the advantages of low ammonia volatilization, slow generation of nitrate nitrogen, low nitrogen loss and high nitrogen effectiveness.
Owner:UNIVERSITY OF CHINESE ACADEMY OF SCIENCES

Granular saline-alkali soil conditioner and production method thereof

The invention relates to a granular saline-alkali soil conditioner. The conditioner is prepared from the following raw materials in parts by weight: 70-90 parts of phosphogypsum, 5-15 parts of humic acid and 5-15 parts of filler. The invention also relates to a production method of the saline-alkali soil conditioner. The production method comprises the following steps: preparing the filler, preparing a spray, palletizing, baking, sieving and the like. The granular saline-alkali soil conditioner disclosed by the invention plays a good saline-alkali soil improvement role by combined action of adjusting a plurality of aspects such as the soil pH level and ion components, enhancing the salt resistance ability of crops, activating nutrient elements in soil and the like. The product disclosed by the invention is granular, convenient to use, and convenient for mechanical fertilization. The production method of the product disclosed by the invention has the characteristics that production equipment is low in demands, and just conventional equipment needs to be adopted, special equipment does not need to be added, and the method is wide in raw material source, low in production cost, convenient to transport and fertilize, and the like.
Owner:INST OF AGRI RESOURCES & REGIONAL PLANNING CHINESE ACADEMY OF AGRI SCI

Nano zirconium phosphate-modified triazine macromolecular charring agent, and preparation method and application thereof

The invention discloses a nano zirconium phosphate-modified triazine macromolecular charring agent, and a preparation method and application thereof. The preparation method comprises the following steps: using a silane coupling agent to modify nano zirconium phosphate in an intercalation manner, and preparing an intermediate product through an organic solvent, cyanuric chloride, the silane coupling agent-modified nano zirconium phosphate through intercalation, a diamine monomer and an acid-binding agent; performing in-situ polymerization reaction on the organic solvent, the intermediate product, the diamine monomer and the acid-binding agent to prepare the nano zirconium phosphate-modified triazine macromolecular charring agent. Compared with the prior art, the macromolecular charring agent prepared by the invention is excellent in thermal stability and charring property, has a good synergistic flame-retardant effect with ammonium polyphosphate, and can effectively improve the thermal stability and the compactness of an expandable carbon layer under the high temperature condition, so that the flame-retardant efficiency of an intumescent flame retardant is remarkably improved. A prepared flame-retardant polypropylene material can be widely used in fields of automotive exteriors, furniture, appliances, wires, cables, construction materials and the like.
Owner:SOUTH CHINA UNIV OF TECH

Single-component phosphor-nitrogen double-ring cage-shaped macromolecular intumescent flame retardant as well as preparation method and application thereof

ActiveCN105542160AProximity reactionUniform responsePolymer sciencePolypropylene
The invention discloses a single-component phosphor-nitrogen double-ring cage-shaped macromolecular intumescent flame retardant as well as a preparation method and an application thereof. the preparation method comprises the following steps: at 90-110 DEG C, a nucleophilic substitution reaction is carried out between pentaerythritol and phosphorous oxychloride, and PEPA is obtained; a reaction between PEPA and cyanuric chloride is carried out at -5-10 DEG C for 3-6 hours, a reaction between a product and a diamine compound is carried out at 50-60 DEG C for 5-10 hours, and then a reaction between the product and the diamine compound is carried out at 90-110 DEG C for 5-10 hours; finally the single-component phosphor-nitrogen double-ring cage-shaped macromolecular intumescent flame retardant is obtained for flame retardant modification of polymers. Compared with the prior art, the prepared single-component macromolecular intumescent flame retardant has the advantages of high flame retardation efficiency, good compatibility with polymers, etc.; the intumescent flame retardant whose weight is 20-25 wt% of polypropylene can be added into the polypropylene for endowing the polypropylene with good flame retardation performance, and the intumescent flame retardant can be widely applied to the fields of internal and external decorative parts of automobiles, furniture and electric appliances, wires and cables, building material, etc.
Owner:SOUTH CHINA UNIV OF TECH

Preparation method of magnetic-functionalized graphene composite material

The invention provides a preparation method of a magnetic-functionalized graphene composite material, and relates to preparation of a graphene composite material. According to the invention, the preparation method is simple, the raw material is easily obtained, and the industrial production is easy; the prepared magnetic-functionalized graphene composite material has superparamagnetic property and is higher in saturated magnetization; and the graphene carrier is good in conductivity, and loaded ferroferric oxide nano particles are uniformly distributed, are small and are good in crystallizability. The preparation method comprises the following steps of: matching ethanediamine and water into a mixed solvent, then ultrasonically dispersing graphite oxide and iron acetylacetonate in the mixed solvent, and obtaining ethanediamine/dispersion of the graphite oxide and the iron acetylacetonate; transferring the ethanediamine/dispersion of the graphite oxide and the iron acetylacetonate into a reactor lined with polytetrafluoroethylene for reaction and obtaining solid products; and cleaning the solid products, collecting the products with a magnet, drying and obtaining the magnetic-functionalized graphene composite material.
Owner:XIAMEN FUNANO NEW MATERIAL TECH COMPANY

Method for removing sulfur from waste lead-acid storage battery gypsum mud by using magnesium chloride

The invention relates to a method for removing sulfur from waste lead-acid storage battery gypsum mud by using magnesium chloride, which is characterized by comprising the following steps of: firstly, decomposing a waste lead storage battery subjected to acid pouring to obtain the gypsum mud, and entering the next process for later treatment; then leaching the gypsum mud by using a magnesium chloride solution, converting lead sulfate in the gypsum mud into lead chloride entering into the solution, leaving other oxides of lead in leached slag, carrying out liquid-solid separation after leaching is ended, and smelting the leached slag at the low temperature to produce wet lead; cooling to crystallize a leachate to obtain solid lead chloride and crystallized mother liquor, smelting the solid lead chloride at low temperature to produce the wet lead, carrying out regeneration treatment on the crystallized mother liquor by using the crystallized mother liquor and then returning to the step of desulfurizing and leaching the gypsum mud; and finally, adding calcium chloride to the crystallized mother liquor to regenerate the magnesium chloride as a desulfurizing agent and simultaneously produce calcium sulfate as a byproduct. The invention has good desulfurizing effect, and the magnesium chloride as the desulfurizing agent has low price, is easy to regenerate and can be recycled. The invention does not have high requirement on production equipment, greatly reduces the production cost and has obvious advantages.
Owner:SHENYANG RES INST OF NONFERROUS METALS

Method for preparing nanoscale sheet cerium oxide by hydrothermal method

The invention discloses a method for preparing nanoscale sheet cerium oxide by a hydrothermal method. The method comprises the following steps of: 1) preparing a 0.01-0.05mol/L Ce<3+> ion aqueous liquor at room temperature; preparing an ammonia water liquor at room temperature, wherein pH value of the ammonia water liquor is greater than 11; 2) placing the ammonia water liquor in a reaction kettle in a temperature range from -10 DEG C to 20 DEG C, taking the Ce<3+> ion aqueous liquor, and slowly dropping to excessive ammonia water liquor while stirring; and 3) stirring the mixed liquor obtained in the step (2) at constant temperature for reacting for 2-24 hours, centrifugalizing after reaction, removing the supernatant liquid, washing the powder obtained by centrifugalization and drying to obtain the solid sheet cerium oxide. According to the method disclosed by the invention, the nanoscale sheet cerium oxide is synthesized by one step by the hydrothermal method. The method is simple in preparation process, and low in demand on production and process conditions. No template materials are required and no organic solvents are added. The method is basically free from pollution and very environmental-friendly.
Owner:ZHEJIANG SCI-TECH UNIV

Method for preparing conducting polymer micro-nanofibers in magnetic spinning mode

The invention discloses a method for preparing conducting polymer micro-nanofibers in a magnetic spinning mode. The method comprises the steps that 1, a magnetic spinning device is built, wherein the magnetic spinning device comprises a rotary collection disc with a permanent magnet; 2, a spinning precursor solution is prepared, wherein magnetic nano particles, high-molecular polymer and conducting polymer are mixed and dissolved in an organic solvent solution; 3, the magnetic spinning device is utilized for preparing conducting polymer micro-nano complex fibers, wherein the spinning precursor solution is injected into a feeding device, the feeding device is started, liquid drops on an opening of a spinning nozzle forms a jet flow under the effect of magnetic field force to be connected with the permanent magnet to be a bridge, a brushless direct-current motor is started to drive the collection disc to rotate, the ferrofluid jet flow is continuously pulled out under the effect of magnetic field force, and conducting polymer micro-nanofibers are wound and formed among vertical supporting columns of the collection disc. The method does not need the high voltage effect, reduces the production cost and potential safety hazards, is suitable for large-scale production and has the good application prospect, and the fibers are distributed in order.
Owner:QINGDAO UNIV

Polystyrene/calcium alginate composite gel microsphere in nuclear shell structure and preparation method thereof

The invention provides a polystyrene/calcium alginate composite gel microsphere in a nuclear shell structure and a preparation method thereof, relating to biopolymer materials. The polystyrene/calcium alginate composite gel microsphere in the nuclear shell structure takes a polystyrene microsphere as a core and calcium alginate gel as a shell, wherein the grain size of the core is 1-100 microns, and the thickness of the shell layer is 50-800 nm. The preparation method comprises the following steps of: mixing polystyrene microsphere with aqueous solution containing a surface active agent I, and carrying out ultrasonic emulsification to obtain mixed solution A; adding sodium alga acid solution in the mixed solution A, and stirring to obtain mixed solution B; adding organic solution containing a surface active agent II into the mixed solution B, and stirring to obtain mixed solution C; adding calcium chloride solution which has the same volume with the sodium alga acid solution into the mixed solution C under stirring to react, and carrying out vacuum filtration, washing the solution until no calcium ion residue exists on the surface and drying to obtain a product D; and dispersing the product D into water, centrifuging the mixture, pouring out supernate and taking out precipitate to obtain the product.
Owner:XIAMEN UNIV

Rare-earth-doped iron-based amorphous thick strip and preparing method thereof

The invention relates to a rare-earth-doped iron-based amorphous thick strip and a preparing method thereof. The component expression of the iron-based amorphous thick strip is FexSiaBbPcYd, wherein x, a, b, c and d are atomic percents of corresponding elements, wherein a is larger than or equal to 0.5 and smaller than or equal to 10, b is larger than or equal to 0.5 and smaller than or equal to 12, c is larger than or equal to 0.5 and smaller than or equal to 8, d is larger than or equal to 0.001 and smaller than or equal to 0.5, and x+a+b+c+d is equal to 100. A plane flow casting method is adopted for manufacturing the strip, during strip manufacturing, a double-line nozzle is adopted, the thickness of the prepared amorphous thick strip ranges from 50 micrometers to 100 micrometers, the lamination coefficient is larger than 0.92, the saturated magnetic induction density is larger than 1.67T. Micro rare earth yttrium is contained in an alloy, the content of impurities of oxygen, sulphur and the like is greatly reduced, and the molten steel mobility is improved; meanwhile the rare earth yttrium improves the amorphous forming capacity of an alloy system, and the amorphous alloy strip with the thickness ranging from 50 micrometers to 100 micrometers can be prepared through the technology method.
Owner:南京腾元软磁有限公司 +3
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