Preparation method of throat clearing preparation
A throat-clearing and preparation technology, which is applied in the field of medicine, can solve problems such as poor stability, unqualified thin-layer identification of salicymus root, and scrapping of materials in batches, so as to improve product stability, detection rate and petogenin content , Improve the effect of curative effect and stability
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Embodiment 1
[0065] Example 1: Weigh 527.5g of nine-headed lion grass, 315g of cinnabar root, 395g of salivarius root, 395g of glutinous rice vine root, 157.5g of golden fruit, 315g of platycodon grandiflorum, 395g of mint and other 7 medicinal materials, divided into 3 equal parts, one part Add 6.7L of water to extract twice, 1 hour each time, combine the extracts, concentrate under reduced pressure, and dry to obtain extract powder 1; add 3.3L of 70% ethanol to extract twice, each time for 1 hour, combine the extracts, and recover the ethanol Concentrate and dry to obtain extract powder 2; add 1.7L of ethyl acetate for ultrasonic extraction twice for 1 hour each time, combine the extracts, recover ethyl acetate, concentrate and dry to obtain extract powder 3, and then add 3 3.8 times the weight of the extract powder was added with polyethylene glycol 4000, heated and melted, and sprayed into menthol ethanol solution (12.5g of menthol was dissolved in 30ml of 75% ethanol), stirred evenly, ...
Embodiment 2
[0066] Example 2: Weigh 527.5g of nine-headed lion grass, 315g of cinnabar root, 395g of salivarius root, 395g of glutinous rice vine root, 157.5g of golden fruit, 315g of platycodon grandiflorum, 395g of mint and other 7 medicinal materials, and divide them into 3 equal parts on average. Add 8.3L of water to extract twice, 1 hour each time, combine the extracts, concentrate under reduced pressure, and dry to obtain extract powder 1; add 5L of 70% ethanol to extract twice, each time for 1 hour, combine the extracts, recover ethanol and Concentrate and dry to obtain extract powder 2; add 2.5L of ethyl acetate for ultrasonic extraction twice, each time for 1 hour, combine the extracts, recover ethyl acetate, concentrate and dry to obtain extract powder 3, and then add 3 parts Mix the extract powder evenly, add polyethylene glycol 4000 in an amount of 4 times the weight of the extract powder, heat and melt, spray 25ml of peppermint oil, stir evenly, and drop into pills.
Embodiment 3
[0067] Example 3: Weigh 527.5g of nine-headed lion grass, 315g of cinnabar root, 395g of salivarius root, 395g of glutinous rice vine root, 157.5g of golden fruit, 315g of platycodon grandiflorum, 395g of mint and other 7 medicinal materials, and divide them into 3 equal parts on average. Add 6.7L of water to extract twice, 2 hours each time, combine the extracts, concentrate under reduced pressure, and dry to obtain extract powder 1; add 3.3L of 65% ethanol to extract twice, each time for 2 hours, combine the extracts, and recover the ethanol Concentrate and dry to obtain extract powder 2; add 1.7L of ethyl acetate for ultrasonic extraction twice for 2 hours each time, combine the extracts, recover ethyl acetate, concentrate and dry to obtain extract powder 3, and then add 3 The extract powder is mixed evenly, 12.5 grams of menthol is added, the mixture is evenly mixed, an appropriate amount of starch is added, and the capsules are ready.
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