Preparation process of high-performance fiber three-phase composite material
A high-performance fiber and composite material technology, applied in carbon fiber, fiber processing, textiles and papermaking, etc., can solve the problems of low interface bonding strength and insufficient mechanical properties, and achieve the effect of improving mechanical properties, easy bonding, and enhancing bonding strength.
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[0022] The preparation process of high-performance fiber three-phase composite material comprises the following steps:
[0023] First, 5g of carbon fiber was added to 400g of concentrated nitric acid at 80°C for 400W ultrasonic oxidation for 5 hours, and then filtered and washed with water until neutral to obtain oxidized carbon fiber.
[0024] Then, disperse 5g of oxidized carbon fiber into 200g of ethoxylated polyethyleneimine solution, the degree of ethoxylation of ethoxylated polyethyleneimine is 80%, heat to 80°C, stir and react for 5 hours, filter and wash with water , and then obtain polyethyleneimine branched carbon fibers.
[0025] Next, immerse the polyethyleneimine branched carbon fiber in 100g of glue solution. The glue solution is prepared by adding 20g of diallyl bisphenol A and 30g of methacrylamide in 150g of ethanol solution, and heating to 60°C Stir the reaction for 4 hours, then evaporate the ethanol to dryness, add 1.2 g of dicumyl peroxide and 8 g of ally...
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