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Preparation process of high-performance fiber three-phase composite material

A high-performance fiber and composite material technology, applied in carbon fiber, fiber processing, textiles and papermaking, etc., can solve the problems of low interface bonding strength and insufficient mechanical properties, and achieve the effect of improving mechanical properties, easy bonding, and enhancing bonding strength.

Pending Publication Date: 2020-10-16
安徽安赛新材料有限公司
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The purpose of the present invention is to provide a high-performance fiber three-phase composite material preparation process, which overcomes the problems of low interfacial bonding strength and insufficient mechanical properties of carbon fiber composite materials in the prior art

Method used

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Examples

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Effect test

Embodiment 1

[0022] The preparation process of high-performance fiber three-phase composite material comprises the following steps:

[0023] First, 5g of carbon fiber was added to 400g of concentrated nitric acid at 80°C for 400W ultrasonic oxidation for 5 hours, and then filtered and washed with water until neutral to obtain oxidized carbon fiber.

[0024] Then, disperse 5g of oxidized carbon fiber into 200g of ethoxylated polyethyleneimine solution, the degree of ethoxylation of ethoxylated polyethyleneimine is 80%, heat to 80°C, stir and react for 5 hours, filter and wash with water , and then obtain polyethyleneimine branched carbon fibers.

[0025] Next, immerse the polyethyleneimine branched carbon fiber in 100g of glue solution. The glue solution is prepared by adding 20g of diallyl bisphenol A and 30g of methacrylamide in 150g of ethanol solution, and heating to 60°C Stir the reaction for 4 hours, then evaporate the ethanol to dryness, add 1.2 g of dicumyl peroxide and 8 g of ally...

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Abstract

The invention discloses a preparation process of a high-performance fiber three-phase composite material, which comprises the following steps: adding carbon fibers into concentrated nitric acid at 80DEG C, carrying out 400W ultrasonic oxidation for 5 hours, filtering, and washing with water to neutrality to obtain oxidized carbon fibers; dispersing the oxidized carbon fibers into an ethoxylated polyethyleneimine solution, heating to 80 DEG C, stirring to react for 5 hours, filtering, and washing with water to obtain polyethyleneimine branched carbon fibers; immersing the polyethyleneimine branched carbon fibers into the glue solution, taking out the polyethyleneimine branched carbon fibers, and then curing the polyethyleneimine branched carbon fibers at 60 DEG C for 1 minute to obtain impregnated fiber; and immediately coating the surface of the impregnated fibers with an ethylene propylene diene monomer layer with the thickness of 20 microns, and curing at 80 DEG C for 5 hours to obtain the three-phase composite material. The preparation process overcomes the defects in the prior art and enhances the interface bonding strength and mechanical properties of the carbon fiber composite material.

Description

technical field [0001] The invention relates to the technical field of high-performance fiber composite materials, and specifically belongs to a preparation process of high-performance fiber three-phase composite materials. Background technique [0002] Carbon fiber is a high-strength and high-modulus fiber with a carbon content of more than 90%. In carbon fiber composite materials, the interface bonding strength between carbon fiber and composite phase is a key factor affecting the mechanical properties of carbon fiber composite materials. Only carbon fiber and composite phase To achieve better interfacial bonding, carbon fibers can effectively transmit external stress, thereby improving the mechanical properties of composite materials. However, due to the small number of surface functional groups and low interfacial bonding strength of carbon fiber, it is difficult to effectively compound with other materials, resulting in the problem of poor overall mechanical properties ...

Claims

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Application Information

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IPC IPC(8): D06M11/64D06M15/61D06M15/227D06M15/285D06M15/347D06M15/327D06M101/40
CPCD06M11/64D06M15/61D06M15/227D06M15/285D06M15/347D06M15/327D06M2101/40
Inventor 马俊杨建军马国栋马亚田
Owner 安徽安赛新材料有限公司
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