Method for adsorbing tetracycline in underground water by using green rust
A tetracycline and groundwater technology, applied in the direction of adsorption water/sewage treatment, contaminated groundwater/leachate treatment, chemical instruments and methods, etc., can solve the problems of ecological system damage, endangering human life and health, and achieve the effect of ensuring safety
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Embodiment 1
[0015] A method for patina to adsorb tetracycline in groundwater. In an anaerobic incubator, add 8 mL of TC solution with an initial concentration of 5 mg / L and GR of 2 g / L to an 8 mL brown extraction bottle. Close the bottle cap tightly and place it on a QB-328 rotary incubator to rotate in the dark at a speed of 45r / min. Samples are taken regularly. All samples are separated from solid and liquid through a 0.45 μm filter membrane to realize the adsorption of tetracycline. The water samples obtained from solid-liquid separation were analyzed by high-performance liquid chromatography.
[0016] In this embodiment, green rust (GR) can effectively adsorb TC in groundwater. figure 1 is the effectiveness of GR in adsorbing TC in water. The dosage of GR was 2g / L, the initial concentration of TC was 5mg / L, and the removal rate of TC adsorbed by GR was about 97% after 12 hours of reaction. figure 2 is the efficiency of GR to adsorb TC in water under different GR dosages. After 12 ...
Embodiment 2
[0018] In an anaerobic incubator, add 8 mL of TC solution with an initial concentration of 1 mg / L and 0.5 g / L of GR to an 8 mL brown extraction bottle respectively, tightly cap the bottle and place it on a QB-328 rotary incubator at 30 r / min The rotation speed was protected from light, and the reaction was carried out for 12 hours. All the samples were separated from the solid and liquid through a filter membrane of 0.45 μm, and the removal rate of tetracycline was 99.4%.
Embodiment 3
[0020] In an anaerobic incubator, add 8mL of TC solution with an initial concentration of 80mg / L and 8g / L of GR to an 8mL brown extraction bottle respectively, tightly cap the bottle and place it on a QB-328 rotary incubator at a speed of 70r / min. The rotating speed was protected from light, and the reaction was carried out for 12 hours. All the samples were separated through a 0.45 μm filter membrane for solid-liquid separation, and the removal rate of tetracycline reached 66.2%.
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