Fresh and sweet type vetiver root composite extract for cigarettes and application thereof
A technology of compound extract and vetiver root, applied in tobacco, application, preparation of tobacco, etc., can solve rare problems, achieve synergistic effects, reduce second-hand smoke odor, and reduce smoke odor
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Embodiment 1
[0025] A kind of sweet-flavor type vetiver root composite extract for cigarettes, prepared as follows:
[0026] (1) Weigh 80 kg of fresh and dried Vetiver root, 1 Kedilo pulp, 0.2 Zheer root, 0.3 Chinensis root, 0.2 Reed root, 0.3 Pueraria root, 0.5 bellflower root, 0.2 lemon peel, 0.2 orange flower, and 0.3 licorice. , crush all the materials and pass through a 20-mesh sieve, and put them into the ultrasonic extraction tank; then add petroleum ether to the ultrasonic extraction tank according to the mass ratio of material to liquid 1:12 and stir and mix, that is, the mass ratio of crushed materials to petroleum ether is 1:12 , ultrasonic extraction was carried out 4 times, and the conditions of ultrasonic extraction were: temperature 25°C, ultrasonic power 400W, space ratio 70%, ultrasonic frequency 20KHz, time 20min. Ultrasonic extraction can better dissolve the effective semi-volatile components in the raw materials, and adding a solvent helps to effectively dissolve the fa...
Embodiment 2
[0034] A kind of sweet-flavor type vetiver root composite extract for cigarettes, prepared as follows:
[0035] (1) Weigh 100 kg of fresh and dried Vetiver root, 10 kg of Kedilo pulp, 5 kg of Zheer root, 5 kg of Chine root, 5 kg of reed root, 5 kg of Pueraria root, 5 kg of Bellflower root, 5 kg of lemon peel, 5 kg of orange 5 kg of flowers and 10 kg of licorice, crush all the materials and pass through a 40-mesh sieve, and put them into the ultrasonic extraction tank; then add ethyl acetate to the ultrasonic extraction tank according to the mass ratio of material to liquid 1:10 and stir and mix, and perform ultrasonic extraction 5 times , the conditions of ultrasonic extraction are: temperature 18°C, ultrasonic power 1000W, ultrasonic frequency 20KHz, duty ratio 80%, and time 30min.
[0036] (2) Filtrate the ultrasonically extracted product, combine the filtrates to distill under reduced pressure, concentrate until the volume is about 1 / 13 of the original volume of the filtrat...
Embodiment 3
[0043] A kind of sweet-flavor type vetiver root composite extract for cigarettes, prepared as follows:
[0044] (1) Weigh 50 kg of fresh and dried Vetiver root, 0.15 kg of Kedilo pulp, 0.1 kg of Zheer root, 0.1 kg of Chinensis root, 0.1 kg of reed root, 0.1 kg of Pueraria root, 0.1 kg of Campanulaceae, 0.1 kg of lemon peel, 0.1 kg of orange 0.1 kg of flowers and 0.1 kg of licorice, all the materials were crushed and passed through a 60-mesh sieve, and put into the ultrasonic extraction tank; then acetone was added to the ultrasonic extraction tank according to the mass ratio of material to liquid 1:15 and stirred and mixed, ultrasonic extraction was carried out 3 times, and ultrasonic extraction The extraction conditions are: temperature 0°C, ultrasonic power 40W, ultrasonic frequency 20KHz, duty ratio 60%, and time 40min.
[0045] (2) Filtrate the ultrasonically extracted product, combine the filtrates to distill under reduced pressure, concentrate until the volume is 1 / 20 of...
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