Preparation method of composite hollow reflecting layer
A reflective layer and hollow technology, which is used in the preparation of composite hollow reflective layers, can solve problems such as poor thermal stability and printing ink gelatinization, and achieve the effects of improving pressure resistance, reducing side loss, and ensuring connection stability
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Embodiment 1
[0019] The invention relates to a composite hollow reflective layer, which uses polypropylene hollow microspheres as hollow balls and multifunctional cage polysilsesquioxane as an adhesive linker to form a composite hollow reflective layer.
[0020] There are 6 functional groups in the multifunctional cage polysilsesquioxane, and the functional groups are chlorine groups; the hollow ratio of the polypropylene hollow microspheres is 40%.
[0021] The preparation method of the composite hollow reflective layer comprises the following steps:
[0022] Step 1: Add dimethyldiethoxysilane to 1L of toluene for low-temperature ultrasonic dispersion to form a solution, then spray the solution evenly on the surface of polypropylene hollow microspheres to form a liquid film, and let it stand for 10 minutes to obtain a wet film microsphere. ball; the concentration of the dimethyldiethoxysilane in toluene is 100g / L, the temperature of the low-temperature ultrasonic dispersion is 5°C, the ul...
Embodiment 2
[0028] The invention relates to a composite hollow reflective layer, which uses polypropylene hollow microspheres as hollow balls and multifunctional cage polysilsesquioxane as an adhesive linker to form a composite hollow reflective layer.
[0029] The functional groups in the multifunctional cage polysilsesquioxane contain 8, and the functional groups are chlorine groups; the hollow ratio of the polypropylene hollow microspheres is 50%.
[0030] The preparation method of the composite hollow reflective layer comprises the following steps:
[0031] Step 1: Add dimethyldiethoxysilane to 1L of toluene for low-temperature ultrasonic dispersion to form a solution, then spray the solution evenly on the surface of polypropylene hollow microspheres to form a liquid film, and let it stand for 20 minutes to obtain a wet film microsphere. ball; the concentration of the dimethyldiethoxysilane in toluene is 300g / L, the temperature of the low-temperature ultrasonic dispersion is 10°C, the...
Embodiment 3
[0037] The invention relates to a composite hollow reflective layer, which uses polypropylene hollow microspheres as hollow balls and multifunctional cage polysilsesquioxane as an adhesive linker to form a composite hollow reflective layer.
[0038] The functional groups in the multifunctional cage polysilsesquioxane contain 7, and the functional groups are chlorine groups; the hollow ratio of the polypropylene hollow microspheres is 45%.
[0039] The preparation method of the composite hollow reflective layer comprises the following steps:
[0040] Step 1: Add dimethyldiethoxysilane to 1L of toluene for low-temperature ultrasonic dispersion to form a solution, and then spray the solution evenly on the surface of polypropylene hollow microspheres to form a liquid film, and let it stand for 15 minutes to obtain a wet film microsphere. ball; the concentration of dimethyldiethoxysilane in toluene is 200g / L, the temperature of low-temperature ultrasonic dispersion is 8°C, the ultr...
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