Heat-conducting gasket and preparation method thereof
A technology for thermally conductive gaskets and thermally conductive fillers, which is applied to chemical instruments and methods, flat products, heat exchange materials, etc., can solve the problems of increased application thermal resistance, change of orientation of thermally conductive fillers, large-scale, low degree of continuity, etc. Achieve the effects of improved thermal conductivity, reduced application thermal resistance, and excellent mechanical properties
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[0039] An exemplary method for preparing a thermal pad of the present invention generally includes the following steps:
[0040] (1) After mixing the binder, the two-dimensional thermally conductive filler and other optional components, and optionally vacuum defoaming, a mixed material is obtained;
[0041] (2) extruding the mixed material into a sheet through a split-combination die head;
[0042] (3) The sheet is drawn, calendered and vulcanized to obtain the thermal pad.
[0043] As the binder of the present invention, it can be selected from at least one of thermosetting resins, thermoplastic resins, thermoplastic elastomers or mixtures thereof.
[0044] The thermosetting resin is selected from at least one crosslinking resin, such as epoxy resin, phenolic resin, silicone resin, polyurethane, polyimide resin, unsaturated polyester, polymethylsiloxane, maleamide At least one of resin, thermosetting polyphenylene ether, melamine formaldehyde resin, furfural phenol resin, fur...
Embodiment 1
[0104] In the present embodiment, each component that adopts is as follows:
[0105] Binder: two-component addition type liquid silicone;
[0106] Two-dimensional thermally conductive filler: graphite, with a sheet diameter of 50-150 μm and a thickness of 1-5 μm;
[0107] Isotropic thermally conductive filler: alumina, with an average particle size of 20 μm;
[0108] Catalyst: platinum catalyst;
[0109] The preparation and implementation process is as follows:
[0110] (1) The raw materials of each component are uniformly mixed according to the following mass parts ratio:
[0111] Two-component addition type liquid silica gel: 145 parts by mass (14.5wt.%)
[0112] Graphite: 550 parts by mass (55wt.%)
[0113] Aluminum nitride powder: 300 parts by mass (30wt.%)
[0114] Platinum catalyst: 5 parts by mass (0.5wt.%)
[0115] (2) After the above-mentioned mixed material is vacuum removed, it is placed in an extrusion device, extruded into sheets through a split-combination...
Embodiment 2
[0124] In the present embodiment, each component that adopts is as follows:
[0125] Binder: two-component addition type liquid silicone;
[0126] Two-dimensional thermally conductive filler: graphene, with a sheet diameter of 5-30 μm and a layer number of 1-10;
[0127] Isotropic thermally conductive filler: alumina, average particle size 100μm, 50μm, 5μm, mass ratio 100μm:50μm:5μm=5:3:2;
[0128] Catalyst: Platinum Catalyst
[0129] The preparation and implementation process is as follows:
[0130] (1) The raw materials of each component are uniformly mixed according to the following mass parts ratio:
[0131] Two-component addition type liquid silica gel: 145 parts by mass (14.5wt.%)
[0132] Graphene: 450 parts by mass (45wt.%)
[0133] Alumina: 400 parts by mass (40wt.%)
[0134] Platinum catalyst: 5 parts by mass (0.5wt.%)
[0135] (2) After the above-mentioned mixed material is vacuum removed, it is placed in an extrusion device for extrusion. The material flows ...
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