Dual-wavelength infrared anti-forgery ink and preparation method thereof
An anti-counterfeit ink and dual-wavelength technology, which can be used in inks, household utensils, applications, etc., can solve the problems of single, low anti-counterfeiting ability, and easy preparation
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Embodiment 1
[0032] A dual-wavelength infrared anti-counterfeiting ink, comprising the following components by weight percentage: infrared anti-counterfeiting material 1: 3.5wt%, infrared anti-counterfeiting material 2: 0.75wt%, linking material: 1wt%, pigment 8wt%, auxiliary agent 30wt%;
[0033] The main component of the infrared anti-counterfeiting material one is YLiF 4 :Tm 3+ 、YLiF 4 :Yb 3+ 、YiF 4 :Ho 3+ 、NaYF 4 :Tm 3+ 、NaYF 4 :Yb 3+ 、NaYF 4 :Ho 3+ More than one of them; the preparation method of the infrared anti-counterfeiting material one is: Y 2 o 3 , LiF, NH 4 HF 2 、Er 2 o 3 、Tm 2 o 3 , Yb 2 o 3After mixing evenly in proportion, adjust the pH value of the solution: 2 to 5, put it into a polytetrafluoroethylene container, and then put it into a high-pressure reactor, react at 220°C for 4 to 5 days, and prepare it by suction filtration, washing, and drying. have to.
[0034] The second infrared anti-counterfeiting material is a compound with the following gener...
Embodiment 2
[0049] The dual-wavelength infrared anti-counterfeiting ink comprises the following components by weight percentage: infrared anti-counterfeiting material 1: 4.5wt%, infrared anti-counterfeiting material 2: 2wt%, linking material: 95wt%, pigment 30wt%, auxiliary agent 25wt%; said linking material , including the following components by weight percentage: (a) resin 15%, (b) solvent 55%, (c) vegetable oil 60%, (d) reactive diluent 2%. Wherein, (a) the resin is an alkylphenol phenolic resin; (b) the vegetable oil is linseed oil; the pigment is transparent varnish; and the auxiliary agent is carnauba wax.
[0050] The preparation method of infrared anti-counterfeiting material 1, the preparation method of infrared anti-counterfeiting material 2, and the preparation method of dual-wavelength infrared anti-counterfeiting ink are the same as in Example 1.
Embodiment 3
[0052] Dual-wavelength infrared anti-counterfeiting ink, including the following components by weight percentage: infrared anti-counterfeiting material 1: 4.0wt%, infrared anti-counterfeiting material 2: 1.8wt%, linking material: 85wt%, pigment 20wt%, auxiliary agent 25wt%; The material includes the following components by weight percentage: (a) resin 25%, (b) solvent 50%, (c) vegetable oil 70%, (d) reactive diluent 15%. Wherein, (a) the resin is an unsaturated polyester resin; (b) the vegetable oil is castor oil; the pigment is golden red; the auxiliary agent is carnauba wax.
[0053] The preparation method of infrared anti-counterfeiting material 1, the preparation method of infrared anti-counterfeiting material 2, and the preparation method of dual-wavelength infrared anti-counterfeiting ink are the same as in Example 1.
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