Environment-friendly efficient boiler water regulator for drum boiler
A technology of steam drum boiler and water conditioner, which is applied in natural water treatment, descaling and water softening, non-polluted water treatment, etc., and can solve problems such as soil loss, endangering human life and health, and accidental ingestion
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Synthetic example 1
[0032] (1) Add 15g of lauryl acrylate, 5g of isobornyl acrylate, 7g of cyclohexyl acrylate, 3g of hydroxyethyl acrylate, 15g of N,N-dimethylaminoethyl methacrylate, 15g of diacrylate Methylaminoethyl ester and 0.3g of the initiator AIBN are mixed evenly to obtain the solution to be added dropwise, and set aside;
[0033] (2) add the mixed solvent that is made up of the ethyl acetate of 60g and the toluene of 60g in the reactor, after the system is warmed up to 70 ℃, start to drop the solution to be added dropwise;
[0034] (3) After the uniform dropwise addition is completed within 3 hours, after heat preservation and aging at 70°C for 2 hours (infrared absorption spectrum shows 1640cm -1 The absorption peak disappears) the reaction is complete;
Synthetic example 2
[0036] (1) 7g of isooctyl acrylate, 3g of hydroxyethyl acrylate, 20g of decyl acrylate, 20g of N,N-dimethylaminoethyl methacrylate, 10g of acrylamide and 0.5g of initiator AIBN Mix evenly to obtain the solution to be added dropwise, and set aside;
[0037] (2) add the mixed solvent that is made up of the ethyl acetate of 60g and the toluene of 60g in the reactor, after the system is warmed up to 70 ℃, start to drop the solution to be added dropwise;
[0038] (3) After uniform dropwise addition within 4 hours, heat preservation and aging at 70°C for 2 hours (infrared absorption spectrum shows 1640cm -1 The absorption peak disappears) the reaction is complete;
[0039] (4) After concentrating the reaction solution in step (3) under reduced pressure, carry out gradient elution with a mixed solvent composed of n-hexane and ethyl acetate (the gradient elution method is the same as in Example 1), to obtain the organic amine polymer 2. The molecular weight measured by GPC is 13770,...
Synthetic example 3
[0041] (1) 20g of decyl acrylate, 7g of isobornyl acrylate, 3g of hydroxyethyl acrylate, 4g of N,N-dimethylaminoethyl methacrylate, 4g of dimethylaminoethyl acrylate and 0.2g The initiator AIBN is mixed evenly, obtains the solution to be added dropwise, for subsequent use;
[0042] (2) add the mixed solvent that is made up of the ethyl acetate of 38g and the toluene of 38g in the reactor, after the system is warmed up to 70 ℃, start to drop the solution to be added dropwise;
[0043](3) After the uniform dropwise addition is completed within 6 hours, heat preservation and aging at 70°C for 2 hours (infrared absorption spectrum shows 1640cm -1 The absorption peak disappears) the reaction is complete;
[0044] (4) After concentrating the reaction solution in step (3) under reduced pressure, carry out gradient elution with a mixed solvent consisting of n-hexane and ethyl acetate (the gradient elution method is the same as in Example 1).
[0045] The obtained organic amine polym...
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