Shape memory alloy hollow micro-lattice material and preparation method thereof

A technology of memory alloy and micro-lattice, which is applied in the field of micro-lattice materials to achieve the effects of good film uniformity, wide selection of materials, and good memory effect

Inactive Publication Date: 2021-12-31
XI AN JIAOTONG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] As the performance requirements of materials in aerospace, energy, chemical and biomedical fields are getting higher and higher, people pay more and more attention to low-density materials; micro-lattice materials have excellent mechanical properties and high Designability and extraordinary versatility; through the optimal design of the geometric configuration of the micro-lattice material unit structure, the multi-level sub-scale of the structural elements of the material can be adjusted to achieve the unity of low density and high strength of the material, and its elastic modulus The weight and strength are far superior to other ultra-light materials such as carbon nanotubes, graphene, metal foam and silicon aerogel with the same density. It breaks through the performance limitations of disordered structures and is a promising future Structurally efficient materials; NiTi shape memory alloy materials are attracting more and more attention because of their excellent superelasticity, recoverability and biocompatibility; porous NiTi shape memory alloys are good energy absorbing materials, compared to solid point The hollow lattice material has the characteristics of light weight, high specific strength, and high specific energy absorption; using NiTi shape memory alloy material as the matrix material of the hollow lattice material can obtain a more lightweight, structure-function integrated Micro-lattice materials; therefore, there are certain requirements for some NiTi shape-memory alloy hollow micro-lattice materials and their preparation methods in the market; however, there is no NiTi material with strong designability, simple and easy preparation method. Shape memory alloy hollow micro-lattice material; therefore, it is very necessary to invent a shape memory alloy hollow micro-lattice material and its preparation method at this stage

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  • Shape memory alloy hollow micro-lattice material and preparation method thereof
  • Shape memory alloy hollow micro-lattice material and preparation method thereof
  • Shape memory alloy hollow micro-lattice material and preparation method thereof

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Effect test

Embodiment 1

[0021] A shape-memory alloy hollow micro-lattice material, the formula includes: NiTi alloy with equiatomic ratio, and the weight percentage of the component is: 100% NiTi alloy.

[0022] A method for preparing a shape memory alloy hollow micro-lattice material, comprising step 1, polymer mask processing; step 2, NiTi alloy film layer sputtering forming; step 3, hollow micro-lattice material acquisition; step 4, having memory Effect of NiTi alloy hollow micro-lattice material acquisition;

[0023] In the above step 1, first establish a micro-array material model with a relative density of 5% and a unit rod diameter of 0.1mm through CAD software, then convert the CAD file into an STL format file, and then import the STL format file into the 3D printing device , using digital light processing technology to process PR48 photosensitive resin octahedral micro-lattice material mask; the process parameters are projection resolution 768×480, projection light band 350nm, slice thicknes...

Embodiment 2

[0028] A shape-memory alloy hollow micro-lattice material, the formula includes: NiTi alloy, and the weight percentage of the component is: 100% NiTi alloy.

[0029] A method for preparing a shape memory alloy hollow micro-lattice material, comprising step 1, polymer mask processing; step 2, NiTi alloy film layer sputtering forming; step 3, hollow micro-lattice material acquisition; step 4, having memory Effect of NiTi alloy hollow micro-lattice material acquisition;

[0030] In the above step 1, first establish a micro-array material model with a relative density of 10% and a unit rod diameter of 0.2mm through CAD software, then convert the CAD file into an STL format file, and then import the STL format file into the 3D printing device , using digital light processing technology to process composite EX-200 photosensitive resin material face-centered cube micro-lattice material mask; process parameters are ultraviolet laser 355nm, scanning speed 300mm / s, scanning distance 0.3...

Embodiment 3

[0035] A shape-memory alloy hollow micro-lattice material, the formula includes: NiTi alloy, and the weight percentage of the component is: 100% NiTi alloy.

[0036] A method for preparing a shape memory alloy hollow micro-lattice material, comprising step 1, polymer mask processing; step 2, NiTi alloy film layer sputtering forming; step 3, hollow micro-lattice material acquisition; step 4, having memory Effect of NiTi alloy hollow micro-lattice material acquisition;

[0037] In the above step 1, first establish a micro-array material model with a relative density of 5% and a unit rod diameter of 0.1mm through CAD software, then convert the CAD file into an STL format file, and then import the STL format file into the 3D printing device , using digital light processing technology to process composite EX-200 photosensitive resin material rhombic dodecahedron micro-lattice material mask; process parameters are ultraviolet laser 355nm, scanning speed 300mm / s, scanning distance 0....

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Abstract

The invention discloses a shape memory alloy hollow micro-lattice material and a preparation method thereof. The formula comprises an equal atomic ratio of NiTi alloy, and the weight percentage of the component is 100% of NiTi alloy. The preparation method comprises the following steps of: step 1, polymer mask processing; step 2, NiTi alloy film sputtering forming; step 3, hollow micro-lattice material obtaining; and step 4, NiTi alloy hollow micro-lattice material obtaining with a memory effect. The hollow micro-lattice material prepared by the preparation method disclosed by the invention is high in structural designability; the method for obtaining the shape memory alloy hollow micro-lattice material is simple, convenient and easy to implement, and the thickness of a film can be controlled by controlling the sputtering time, so that the regulation and control of the thickness of a tube wall between 50nm and 20 microns can be realized; the micro-lattice material prepared by the preparation method disclosed by the invention has the advantages of light weight, superelasticity, outstanding memory effect, high damping, energy absorption and biocompatibility; and compared with other deposition methods, the preparation method disclosed by the invention has the advantages of wide material selection and better film uniformity by using a magnetron sputtering technology.

Description

technical field [0001] The invention relates to the technical field of micro-lattice materials, in particular to a shape-memory alloy hollow micro-lattice material and a preparation method thereof. Background technique [0002] As the performance requirements of materials in aerospace, energy, chemical and biomedical fields are getting higher and higher, people pay more and more attention to low-density materials; micro-lattice materials have excellent mechanical properties and high Designability and extraordinary versatility; through the optimal design of the geometric configuration of the micro-lattice material unit structure, the multi-level sub-scale of the structural elements of the material can be adjusted to achieve the unity of low density and high strength of the material, and its elastic modulus The weight and strength are far superior to other ultra-light materials such as carbon nanotubes, graphene, metal foam and silicon aerogel with the same density. It breaks ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C19/03C23C14/20C23C14/35C23C14/58C21D1/26C22F1/02C22F1/10
CPCC22C19/03C22C19/007C23C14/205C23C14/35C23C14/0005C23C14/5873C21D1/26C22F1/02C22F1/006C22F1/10
Inventor 王永静吴雨豪朱晓东陈亚奇
Owner XI AN JIAOTONG UNIV
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