Skin-whitening and freckle-removing purple perilla essential oil and extraction method of extract
A perilla essential oil and extraction method technology, which is applied in the field of extraction of perilla essential oil and extract, can solve the problems of large solvent consumption and incomplete extraction, and achieve the effects of saving extraction time, retaining activity, and high retention rate
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Embodiment 1
[0041] Grinding perilla to a particle size of 0.5-1mm;
[0042] Put the perilla powder into the solid storage tank of the Soxhlet extractor, the solvent ratio is ethanol to water 1:1, the extraction agent ratio is solvent to perilla 1:1, and reduce pressure at 0.02-0.03Mpa at 40°C Distilled, siphoned 5 times.
[0043] Filter with 300 mesh sieve;
[0044] 0.02-0.03Mpa, the solvent is distilled off under reduced pressure at 40°C;
[0045] 0.02Mpa, fractional distillation at 25°C, the low boiling point fraction is essential oil, and the high boiling point fraction is extract.
Embodiment 2
[0047] Grinding perilla to a particle size of 0.5-1mm;
[0048] Put the perilla powder into the solid storage tank of the Soxhlet extractor, the solvent ratio is ethanol to water 2:1, the extraction agent ratio is solvent to perilla 1.5:1; and reduce pressure at 0.03-0.04Mpa, 45°C Distilled, siphoned 6 times.
[0049] Filter with 300 mesh sieve;
[0050] 0.03-0.04Mpa, the solvent is distilled off under reduced pressure at 45°C;
[0051] 0.02Mpa, fractional distillation at 25°C, the low boiling point fraction is essential oil, and the high boiling point fraction is extract.
Embodiment 3
[0053] Grinding perilla to a particle size of 0.5-1mm;
[0054] Put the perilla powder into the solid storage tank of the Soxhlet extractor, the solvent ratio is ethanol to water 1:2, the extraction agent ratio is solvent to perilla 2:1 and distill under reduced pressure at 0.04-0.05Mpa at 50°C , siphon 6 times.
[0055] Filter with 300 mesh sieve;
[0056] 0.04-0.05Mpa, the solvent is distilled off under reduced pressure at 50°C;
[0057] 0.02Mpa, fractional distillation at 25°C, the low boiling point fraction is essential oil, and the high boiling point fraction is extract.
[0058] By finally detecting the residue after extraction, it was found that the effect of Example 1 was the best, and the number of times used was the least, indicating that the ratio of 1:1 is the most preferred ratio.
[0059] Compared with the prior art, the extraction method of perilla essential oil and extract of the present invention adopts ethanol and water as solvents in the whole process, wh...
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