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Production process of military diesel oil

A production process, diesel technology, applied in the field of military diesel production technology, can solve the problems of low output of military diesel and inability to produce -35 and -50 military diesel, and achieve the effect of increasing production

Pending Publication Date: 2022-08-02
PETROCHINA CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] However, due to the limitation of reaction tower and diesel fractionation tower production technology, the production process in the related art can only produce No. -10 military diesel oil with higher freezing point, but cannot produce No. -35 and No. -50 military diesel oil with lower freezing point. Resulting in low production of -35 and -50 military diesel

Method used

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  • Production process of military diesel oil
  • Production process of military diesel oil
  • Production process of military diesel oil

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0097] Step 1: Using the atmospheric distillate oil whose physical and chemical properties are shown in Table 1 as the raw material oil, the second distillate oil with a distillation range of 230°C to 300°C is obtained through a diesel fractionator and a diesel stripper.

[0098] Among them, the technological conditions of the diesel fractionation tower are: the pressure at the top of the tower is -38KPa, the temperature at the bottom of the tower is 255°C, and the temperature at the top of the tower is 158°C. The physicochemical properties of the second distillate can be found in Table 2.

[0099] Step 2: Pass the second distillate oil into the reactor, and the reactor is filled with 5A molecular sieve. The physical and chemical properties of the molecular sieve can be seen in Table 3.

[0100] The process conditions of the reactor were as follows: the bed temperature was 290°C, the temperature of the second distillate entering the reactor was 283°C, and the temperature of th...

Embodiment 2~6

[0113] According to the production process in Example 1 and the detection method of military diesel properties, Examples 2 to 6 were carried out. Among them, the physical and chemical properties of molecular sieves in Examples 2 to 6 can be found in Table 5, the production process conditions can be found in Table 6, the physical and chemical properties of the raw oil and the second distillate oil can be found in Table 7, and the physical and chemical properties of the obtained military diesel oil can be found in Table 6 8.

[0114] Table 5 Physical and chemical properties of 5A molecular sieves in Examples 2-6

[0115] project Example 2 Example 3 Example 4 Example 5 Example 6 Bulk bulk density, g / ml 0.73 0.73 0.73 0.71 0.71 Static water absorption, % 22 22 22 22 22 Static n-hexane adsorption, % 14.8 14.8 14.8 15.0 15.0 Packaging water content, % 1.0 1.0 1.0 0.9 0.9

[0116] Production process condition in the emb...

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Abstract

The invention discloses a production process of military diesel oil, and belongs to the technical field of petrochemical engineering. According to the military diesel oil production process provided by the embodiment of the invention, after fractionation is carried out through a diesel oil fractionating tower and steam stripping is carried out through a diesel oil steam stripping tower, dewaxing and pour point depressing are carried out on second distillate oil obtained by the diesel oil steam stripping tower through a molecular sieve; the freezing point of the obtained military diesel oil can be controlled to be below-35 DEG C or below-50 DEG C, so that the yield of military diesel oil No.-35 and No.-50 is increased.

Description

technical field [0001] The present application relates to the technical field of petrochemical industry. In particular, it relates to a production process of military diesel oil. Background technique [0002] Military diesel is mainly used in high-speed diesel engines such as tanks, armored vehicles, and submarines. According to its freezing point, it can be divided into three types: -10, -35 and -50. Compared with ordinary vehicle diesel, military diesel has stricter quality requirements. Military diesel requires moderate viscosity, good evaporation, chemical stability and combustion performance. Therefore, the production process of military diesel is more stringent. [0003] In the related art, when producing military diesel, the feedstock oil is first passed into a reaction tower equipped with a catalyst, and hydrogen is passed into the reaction tower, and the feedstock oil is desulfurized and denitrified by hydrogen. The oil after desulfurization and denitrification i...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10G53/08
CPCC10G53/08C10G2400/04
Inventor 段天平王万真王云波吴超王平吴灵燕马方明刘勇胡冰洁孙长江黄熊伟
Owner PETROCHINA CO LTD