Process for preparing modified bone-glue adhesive
A technology of adhesive and bone glue, which is applied in the preparation of adhesive, animal glue or gelatin, and the type of adhesive, and can solve the problems of high freezing point and slow drying speed of bone glue
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[0004] Below in conjunction with embodiment the present invention is described in further detail:
[0005] The realization method of the present invention is: (1) this reaction is carried out under constant temperature water bath. Weigh 25g of bone glue in a three-neck flask, add 25g of water, stir and dissolve at 60°C; raise the temperature to 80°C, take 2g of sodium hydroxide and add 8-10g of water to make a solution, add it to the mixture of bone glue and water, and degrade it for 0.5h under constant temperature stirring . (2) Cool down to 70°C, add 2g of epichlorohydrin dropwise, and react at constant temperature for 1.5h; during this period, control pH=10-11. (3) Rapidly cool to room temperature, and add 2-8% glue quality drier such as bentonite to obtain a yellow-brown viscous product.
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