Process for preparing dimethyl ether
A dimethyl ether and process technology, applied in the field of dimethyl ether production, can solve the problems of high production cost, poor economy, difficulty in adapting to large-scale production, etc., and achieve the effects of improving market competitiveness and reducing production energy consumption and cost
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[0014] According to the technological process of the present invention, young bituminous coal is used as raw material, multi-nozzle opposed coal-water slurry pressurized gasification furnace, and the quenching process is used for gas production. The coal slurry concentration is 60%-62% (m); the gasification pressure is 5.5-6.5MPa, and the gasification temperature is 1400-1450°C.
[0015] The crude gas produced by gasification is purified by sulfur-resistant shift, MNHD desulfurization, decarbonization and other purification methods to produce synthesis gas that meets the requirements of methanol synthesis. In an air-cooled-water-cooled combined methanol synthesis reactor, methanol is synthesized under a pressure of 4.5-12.0 MPa. The methanol-containing reaction gas undergoes heat recovery and two-stage condensation cooling. The pressure of the condensation cooling system is 3.5-11.0MPa, and the temperature is 30-120°C. The condensate is separated by flash evaporation to obtai...
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