Fluorocopolymer film and its application
A fluorine copolymer and film technology, applied in the field of fluorine copolymer film, can solve problems such as film rupture, and achieve the effects of excellent tear strength or tensile strength, excellent transparency and excellent appearance
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Embodiment 1
[0039] A stirrer-equipped polymerization reactor with an internal volume of 94 liters was degassed. 70.6 kg of 1-hydrotridecafluorohexane, 20.4 kg of 1,3-dichloro-1,1,2,2,3-pentafluoropropane (manufactured by Asahi Glass Company. Limited, hereinafter referred to as AK225cb), 1.89 kg PPVE and 2.25 kg HFP were fed into the polymerization reactor. The temperature inside the polymerization reactor was raised to 66° C., and a TFE / ethylene gas mixture with a molar ratio of 76 / 24 was injected until the pressure reached 1.5 MPa-G. 65 ml of a 1% by mass AK225cb solution of tert-butyl peroxypivalate as a polymerization initiator was charged into the polymerization reactor to initiate the polymerization reaction. The monomer mixture gas of TFE / ethylene=50 / 50 (molar ratio) was continuously fed to keep the pressure constant during the polymerization reaction. 7.3 hours after the initiation of the polymerization reaction, at this time, 7.1 kg of monomer mixed gas was added to lower the te...
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Abstract
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