Method for extracting wine flavour and fragrance substance from yellow water by super critical CO2 technology

A carbon dioxide and supercritical technology, applied in the extraction of flavor and aroma substances for wine, in the field of extracting flavor and aroma substances for wine, can solve the problems of not being suitable for industrialized large-scale production, waste of resources, high production costs, etc., and achieve economical efficiency Excellent, less corrosive, beneficial to extraction

Active Publication Date: 2007-01-24
SICHUAN YIBIN WULIANGYE GROUP +1
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  • Abstract
  • Description
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  • Application Information

AI Technical Summary

Problems solved by technology

[0005] First, it is very uneconomical to not separately extract lactic acid, a substance with high content and high utilization value.
Yellow water contains about 4-8% lactic acid, and 2863.21 mg of lactic acid per 100 ml of yellow water. At present, lactic acid or calcium lactate is widely used in food, flavor and fragrance industries, and is also a good product for the production of food-grade lactic acid or calcium lactate. raw materials, the prior art does not provide technical tips for extracting lactic acid, which causes a waste of resources, and is not ideal from an economic point of view;
[0006] Second, yellow water is highly acidic and highly corrosive to extraction and separation equipment. If it is directly used as the extraction object, it will seriously affect the service life of the equipment;
[0007] Third, this prior art does not design CO 2 recycling step, the CO is directly recovered after the separation step 2 empty, very uneconomical
[0008] The above three reasons are all caused by higher production costs, so this technology is not suitable for the needs of industrialized mass production

Method used

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  • Method for extracting wine flavour and fragrance substance from yellow water by super critical CO2 technology
  • Method for extracting wine flavour and fragrance substance from yellow water by super critical CO2 technology

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Embodiment 1

[0023] Embodiment 1: Utilize supercritical carbon dioxide technology to extract the method for flavor-forming and aroma-forming substance of wine from yellow water, is to carry out as follows:

[0024]Because the yellow water contains a lot of lactic acid bacteria, it can be fermented directly. Take 2000 ml of yellow water and ferment for about 1-3 days. When the total sugar content in the fermented liquid is zero, the fermentation is over, and then add calcium carbonate to neutralize it. Fermented liquid until the pH value of the fermented liquid is 6-8, then filter to remove solid impurities in the fermented liquid, then concentrate the Baumé degree of the fermented liquid to 12-16, put it into a crystallization tank for crystallization, filter and separate crystals and Crystallization mother liquor; then the crystallization mother liquor is sent into the extraction kettle 4, the high-pressure pump 2 is started, the liquid carbon dioxide in the carbon dioxide storage tank 1 i...

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Abstract

The present invention is method of extracting wine flavor and fragrance substance from yellow water as spirit brewing side product and belongs to the field of spirit brewing technology. The extracting process includes the steps of pre-treatment of yellow water, supercritical CO2 extracting, and supercritical CO2 recovering. The present invention has the advantages of capable of extracting lactic acid, full resource utilization, favorable extraction process, less corrosion to the apparatus, etc.

Description

technical field [0001] The invention relates to a method for extracting taste and aroma substances for wine, in particular to a method for extracting taste and aroma substances for wine from yellow water, a by-product of liquor brewing in liquid state, and belongs to the technical field of wine making. Background technique [0002] Liquor is a relatively complex substance system. Through the current analysis methods, it can be analyzed that besides ethanol and water, there are also aroma and taste substances in liquor. More than 200 substances have been detected, mainly including organic acids, Esters, alcohols, carbonyl compounds, phenolic compounds and nitrogen-containing compounds, etc., have very small content in liquor, but have a great impact on the quality of liquor. Their content and proportion determine the aroma and style of liquor, and constitute Aroma and taste of liquor. ("Practical Baijiu Analysis", edited by Cai Dingyu, published by Chen...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C12G3/08
Inventor 王国春陈林赵东李杨华伍运洪邓霞玲
Owner SICHUAN YIBIN WULIANGYE GROUP
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