Cathode for fuel cell and polymer electrolyte fuel cell having same
A fuel cell cathode and polymer technology, applied in the direction of solid electrolyte fuel cells, fuel cells, battery electrodes, etc., can solve the problems of insufficient reduction of cathode overvoltage, insufficient durability of the catalyst layer, lack of oxygen permeability, etc., and achieve excellent Electrode characteristics, increased exchange current density, effect of good electrode characteristics
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example 1
[0066] CeO 2 -ZrO 2 Mixed oxides are used as oxygen absorbing / releasing agents. Printex XE2B was used as the carbon material, and for the platinum material, chloroplatinic acid was supported by carbon by impregnation. CeO loaded with 5wt.% platinum 2 -ZrO 2 A mixed oxide (20 wt.%) was mixed with platinum-supporting carbon to prepare a catalyst.
example 2-1
[0082] Such an electrode is prepared in the following process, the film thickness of the electrode is 3 mil, including a mixed carbon catalyst supporting PtFe (60wt.%) and Ce-Zr-O supporting Pt (5wt.%) x Powder (20wt.%) was pretreated according to the following procedure.
[0083] (1) Ce-Zr-O x The composite oxide powder was dipped into an aqueous solution of dinitrobisamine Pt complex and stirred, then evaporated at 120°C to dry (contains 5 wt.% of Pt relative to the powder)
[0084] (2) After grinding in a mortar, the powder was baked in an atmospheric oven at 500°C for 2 hours, and the powder was ground in a mortar again.
[0085] (3) A commercially available carbon catalyst loaded with PtFe (60wt.%) and a predetermined amount of ion-exchanged water, Ce-Zr-O loaded with Pt 5wt.% x Powder (20 wt.% with respect to the catalyst), electrolyte solution (Nafion), ethanol, and propylene glycol were mixed to obtain a catalyst ink.
[0086] (4) After the catalyst ink was stirred ...
example 2-2
[0091] Such an electrode was prepared with a film thickness of 6 mil, including a mixed carbon catalyst supporting PtFe (30wt.%) and Ce-Zr-O supporting Pt (5wt.%) x Powder (20 wt.%). This example is similar to Example 2-1, but a PtFe (30 wt.%)-supported carbon catalyst was used instead in step (3), and a membrane with a film thickness of 6 mils was used in step (5).
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