Method for extracting natural dye from pomegranate peel and leaft
A technology of pomegranate peel and natural dyes, applied in the field of natural dyes, can solve the problems of complex tannin pigment composition and cannot be directly used as dyes, etc., and achieve the effect of fast dyeing effect
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Embodiment 1
[0025] Take 5 kilograms of pomegranate peel (dry) and 2 kilograms of pomegranate leaves (dry) and put them in a large bottle for extraction (do not use metal containers). Add 35L of 80% ethanol aqueous solution to the pomegranate peel, and add 20L of 70% of the pomegranate leaves. The ethanol aqueous solution was heated for two hours and allowed to stand overnight. Generally 3-4 times of extraction are required until the color becomes lighter. The above extract is filtered and concentrated under reduced pressure. During the concentration of pomegranate leaves, precipitation occurs. Take the precipitate and vacuum dry to obtain a coffee-colored powder; add the concentrate of the pomegranate peel to pure alcohol to obtain a yellow precipitate, which is separated and dried to obtain soil Yellow powder, the mother liquor is concentrated under reduced pressure. Pour the concentrate of the pomegranate peel into a column equipped with a treated macroporous resin adsorption resin for colu...
Embodiment 2
[0032] Take 5 kg of pomegranate peel (dry) and 2 kg of pomegranate leaves (dry) and put them in a large bottle for extraction (do not use a metal container). Add 35L of 50% ethanol aqueous solution to the pomegranate peel, and add 20L of 50% water to the pomegranate leaves. The ethanol aqueous solution was heated for two hours and allowed to stand overnight. Generally 3-4 times of extraction are required until the color becomes lighter. The above extract is filtered and concentrated under reduced pressure. During the concentration of pomegranate leaves, precipitation occurs. Take the precipitate and vacuum dry to obtain a coffee-colored powder; add the concentrate of the pomegranate peel to pure alcohol to obtain a yellow precipitate, which is separated and dried to obtain soil Yellow powder, the mother liquor is concentrated under reduced pressure. Pour the concentrate of the pomegranate peel into a column equipped with a treated macroporous resin adsorption resin for column adso...
Embodiment 3
[0039] Take 5 kg of pomegranate peel (dry) and 2 kg of pomegranate leaves (dry) and put them in a large bottle for extraction (do not use a metal container). Add 35L of 30% ethanol aqueous solution to the pomegranate peel, and add 20L of 30% water to the pomegranate leaves. The ethanol aqueous solution was heated for two hours and allowed to stand overnight. Generally 3-4 times of extraction are required until the color becomes lighter. After filtering the above extract and concentrating under reduced pressure, precipitation occurs during the concentration of pomegranate leaves. Take the precipitate and vacuum dry to obtain a coffee-colored powder; add the concentrate of pomegranate peel to pure alcohol to obtain yellow precipitate, which is separated and dried Yellow powder, the mother liquor is concentrated under reduced pressure. Pour the concentrate of the pomegranate peel into a column equipped with a treated macroporous resin adsorption resin for column adsorption, so that t...
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