On-site analysis system with central processor and method of analyzing
a technology of analysis system and analyzer, applied in chemical methods analysis, instruments, color/spectral property measurement, etc., can solve problems such as the inability of analytical instruments to generate values
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example 1
[0197] A feasibility study was done to determine if a property model could be developed to measure the concentration of squalane in squalene. In accordance with block 70 of FIG. 4, the method was defined as FT-NIR using the MATRIX Model F instrument manufactured by Bruker Optics, with sample presentation for liquid samples provided by closure caps with dimensions of 18-mm diameter×10-mm high manufactured by Cincinnati Container Corporation. The objectives for the property model included measurements of squalane in squalene having concentrations ranging from trace amounts to about 10 weight percent with a limit of desired precision of 0.10% or smaller as measured by RMSEP. The objectives further indicated that the measurements will be taken by non-skilled operators who will dispense about 1 mL of liquid samples into separate, disposable caps, and the sample temperature may vary from about 0° C. to 60° C. In accordance with the block 72 of FIG. 4, the expected range of the concentrati...
example 3
[0204] The orientation of the sample cap is a potentially influential factor (block 84). The orientations are expected to be random. To determine if variation in the orientation of the sample cap (block 86) will affect the predicted concentrations (block 88), a sample of 1.00% of squalane in squalene was prepared and measured with four different cap orientations. The initial orientation of the cap was selected at random, and additional orientations were attained by successively rotating the cap by approximately 90 degrees about an axis perpendicular to the bottom of the cap between measurements. As shown in FIG. 11, measurable differences were observed in these spectra, indicating that orientational variance is probably an influential factor.
[0205] The six calibration samples in the training set of Example 1, each with a sample cap orientation labeled as orientation 1, were then measured with three additional orientations selected at random, labeled as orientations 2, 3, and 4, eac...
example 4
[0209] The sample pathlength for the squalane-squalene mixture, which is twice the distance from the air-liquid interface at the top of the sample volume to the reflective surface of the sample cap at the bottom of the sample, is a potentially influential factor (block 84) since the intensity of the NIR absorbance by the sample is proportional to the sample pathlength. The pathlength for a particular measurement is determined by the dimensions of the cap and the volume of sample dispensed into the cap.
[0210] Additional aspects of the method and objectives of block 70 are now defined. Suppose that the disposable caps of Examples 1 to 3 are to be used as economical sample holders for remote measurements. Since these caps are not manufactured identically, variations in the dimensions of the caps, and hence of the sample pathlength for a uniform volume of material, are inevitable. Further suppose that disposable pipettes with 0.25 mL graduations will be used as economical sample dispen...
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