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Antiseptic wearable oil, sheathed tube liquid nitrogen quenching method

A nitriding treatment, anti-corrosion and wear-resistant technology, which is applied in the direction of metal material coating process, coating, solid-state diffusion coating, etc., can solve the problems of short service life, high cost, and large difference in surface hardness gradient values. Achieve the effects of improved anti-corrosion ability, small hardness gradient and balanced concentration

Inactive Publication Date: 2009-07-22
牛君
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] At present, various series of different forms of oil and casing produced by the existing technology at home and abroad have no anti-corrosion or hardening treatment on the inner and outer surfaces, or only have a single plating, anti-corrosion material or sintered glass lining on the inner surface. However, there are common problems such as low inner surface hardness, poor wear resistance, easy peeling of the surface anti-corrosion layer, resulting in pump jam accidents, polluting the environment and harmful to health, difficult quality assurance, high cost, low strength, and short service life of the product, etc. question
[0003] In the prior art, nitriding technology is also used to treat oil and casing, but the existing technology can only guarantee a good enough nitriding effect for products with a length-to-diameter ratio of less than 30:1, and cannot achieve deep hole nitriding At present, the main problem of deep hole nitriding is that the depth and hardness of the nitrided layer in the middle are very different from those at both ends, and the gradient value of surface hardness is very different.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] Two oil pipes after pretreatment, the oil pipe material is J55, put into the nitriding furnace, the solid nitriding medium is mixed with chromium, titanium and nickel powder in a ratio of 18:1:9, and the parameters of the nitriding furnace are set as follows :

[0031] Voltage 850V; current 60A; vacuum degree 80Pa; solid nitriding medium flux per minute: 5g / min; ammonia gas flux: 2L / min; carbon dioxide flux: 0.12L / min; heating rate 2°C / min; glow Optical thickness 5mm.

[0032] Start heating, when the temperature of the nitriding furnace is 500°C, keep the temperature constant for 6 hours; continue to raise the temperature to 550°C, keep the constant temperature for 6 hours; when the temperature drops to 500°C, keep the constant temperature for 8 hours;

[0033] Test the hardness of the oil pipe: the surface hardness is above 67, 66HRC respectively, and the hardness value at the depth of 1mm reaches 63, 61HRC.

[0034] The anti-corrosion ability is as follows: ordinary...

Embodiment 2

[0037] Two casings after pretreatment, the casing material is N80, are placed in a nitriding furnace, the solid nitriding medium is mixed with titanium and nickel powder in a ratio of 1:1, and the parameters of the nitriding furnace are set as follows:

[0038] Voltage 800V; Current 50A; Vacuum degree 100Pa; Solid nitriding medium per minute throughput: 2.5g / min; Ammonia gas throughput: 3L / min; Carbon dioxide throughput: 0.2L / min; Heating rate: 3°C / min; Glow thickness 4mm.

[0039] Start heating, when the temperature of the nitriding furnace is 450°C, keep the temperature constant for 7 hours; continue to raise the temperature to 550°C, keep the constant temperature for 8 hours; when the temperature drops to 450°C, keep the constant temperature for 7 hours;

[0040] Test the hardness of the casing: the surface hardness is above 66, 65HRC respectively, and the hardness value at the depth of 1mm reaches 63, 62HRC.

[0041] The anti-corrosion ability is: the ordinary untreated o...

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PUM

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Abstract

The invention discloses a nitrogenization processing method that can process an oil pipe or a sleeve with a length diameter ratio being larger than 30 : 1. The method is that: the approximate middle part of an inner hole of the oil pipe or the sleeve is additionally provided with an auxiliary anode, and lifting holes of the oil pipe or the sleeve are arranged at the upper part of a furnace; air inlet devices are arranged on the furnace for every section, and a vacuum vent-hole is arranged at the lower end of the furnace; namely, the invention adopts deep hole nitrogenization technique such as the auxiliary anode and the forced air passing. Furthermore, such metal powders as Cr, Ti, Ni, etc. are added into a nitrogenization media, and three sections of nitrogenizations is adopted, finally a nitrogen seeping layer with a thickness of 0.5-2mm is formed at the surface of the oil pipe and the sleeve, the nitrogen seeping layer can obviously enhance such performances as surface hardness, anti-corrosion ability, abrasion resistance, etc. of the oil pipe or the sleeve, and thus prolonging the service life thereof.

Description

Technical field: [0001] The invention relates to a surface treatment method for oil and casing pipes used in oil fields, in particular to a method for treating the surface of oil and casing pipes using nitriding technology. Background technique: [0002] At present, various series of different forms of oil and casing produced by the existing technology at home and abroad have no anti-corrosion or hardening treatment on the inner and outer surfaces, or only have a single plating, anti-corrosion material or sintered glass lining on the inner surface. However, there are common problems such as low inner surface hardness, poor wear resistance, easy peeling of the surface anti-corrosion layer, resulting in pump jam accidents, polluting the environment and harmful to health, difficult quality assurance, high cost, low strength, and short service life of the product, etc. question. [0003] In the prior art, nitriding technology is also used to treat oil and casing, but the existi...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C23C8/00C23C8/24C23C8/02C23C8/62
Inventor 吕向东朱革陈全刚王国明牛君
Owner 牛君
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