Ester compound and its use in pest control
一种酯化合物、虫害防治的技术,应用在酯化合物及其在虫害防治领域,能够解决杀虫剂活性未必足够等问题
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[0095] The present invention is illustrated in detail by the following Production Examples, Formulation Examples, and Test Examples.
[0096] First, production examples of the compounds of the present invention will be described.
[0097] Production example
[0098]
[0099] Under a nitrogen atmosphere, to 0.50 g of 5-benzyl-3-furylmethanol, 0.62 g of (1R)-cis-2,2-dimethyl-3-((E)-3-ethoxy -2-fluoro-3-oxo-1-propenyl)cyclopropanecarboxylic acid, 0.1g of 4-(dimethylamino)pyridine and 7ml of dichloromethane were added to a mixture of 0.60g of N,N-dicyclohexyl carbon diimine, and the mixture was stirred at room temperature for 3 hours. Then, the reaction mixture was filtered, and the filtrate was concentrated under reduced pressure. The obtained residue was subjected to silica gel column chromatography to obtain 0.69 g of 5-benzyl-3-furylmethyl(1R)-cis-2,2-dimethyl-3-((E)-3- Ethoxy-2-fluoro-3-oxo-1-propenyl)cyclopropanecarboxylate (hereinafter, referred to as the present com...
Embodiment 1
[0104] To a solution of 20 parts of any one of the compounds of the present invention (1) in 65 parts of xylene was added 15 parts of Sorpol 3005X (registered trademark of Toho Chemical Industry Co., LTD.), and the mixture was thoroughly stirred to mix to An emulsifiable concentrate is obtained.
Embodiment 2
[0106] To 40 parts of any one of the compounds of the present invention (1) was added 5 parts of Sorpol 3005X, and the mixture was well stirred and mixed. To the mixture were added 32 parts of Carplex #80 (synthetic hydrated silica, a registered trademark of Shionogi & CO., Ltd.) and 23 parts of 300-mesh diatomaceous earth, and the resulting mixture was thoroughly mixed with a juice mixer to A wettable powder is obtained.
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Abstract
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