Toner for electrostatic charge development, developer using the same, developer cartridge and image forming apparatus
An imaging device, a toner image technology, applied in the direction of developer, electric recording process using charge pattern, equipment for electric recording process using charge pattern, etc., can solve problems affecting printed images, etc., and achieve good readability Effect
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Embodiment 1
[0264]
[0265] 4.0 parts by weight of 2,3-dicyano-1-phenylnaphthalene (the compound represented by the above structural formula (2)), 0.3 parts by weight of vanadyl trichloride, 1.2 parts by weight of 1,8-diazepine as raw materials were mixed. heterobicyclo[5.4.0]-7-undecene and 20 parts by weight of n-aminoalcohol, and then the resulting material was stirred for 6 hours under reflux under heating. After cooling, the resulting mixture was poured into 100 mL of methanol, and the precipitate was filtered off. Next, this precipitate was put into pure water, boiled and washed, and then purified by column chromatography; thereby synthesizing the above "compound represented by structural formula (1)".
[0266] The obtained compound is subjected to an acid paste treatment, thereby being micronized to a desired particle size; thus an infrared absorber A is obtained. Specifically, the process involves dissolving infrared absorber A in 96% concentrated sulfuric acid (120 times the w...
Embodiment 2
[0273]
[0274] Infrared absorbent B was obtained using the same method as in the case of infrared absorbent A except that ultimizer treatment was performed instead of acid paste treatment as pulverization treatment. (Specifically, using Ultimizer-HJP-2500, under a pressure of 230 MPa, 20Pass treatment was carried out to an aqueous solution of 10% by weight of an infrared absorber and 10 parts by weight of a dispersant (trade name: Newlex Paste H, manufactured by NOF Corporation) ( 32 minutes); thus obtained particles.)
[0275] The volume average particle diameter of the infrared absorber B thus obtained was 0.32 μm.
[0276]
[0277] Toner B was obtained using the same method as in producing Toner A except that Infrared Absorber B was used instead of Infrared Absorber A.
Embodiment 3
[0292]
[0293] 0.5 parts by weight of the above-mentioned infrared absorber "VONPc-Ph" (manufactured by Sigma-Aldrich Inc.), 0.5 parts by weight of anionic surfactant (dodecylbenzenesulfonic acid) and 99 parts by weight of ion-exchanged water were mixed, and homogenized (trade name: Ultratalux T50, manufactured by IKA Co., Ltd.) was used to disperse the resulting solution for 10 minutes, and then dispersed using a circulating ultrasonic dispersion device (trade name: RUS-600TCVP, manufactured by Nippon Seiki Seisakusho); as a result, Infrared absorber dispersion A'.
[0294] The volume average particle diameter of the infrared absorber obtained in the infrared absorber dispersion A' was 0.13 µm, and the solid content ratio of the infrared absorber was 0.5% by weight.
[0295]
[0296] Put 65 parts by weight of dimethyl adipate, 183 parts by weight of dimethyl terephthalate, 223 parts by weight of bisphenol A-ethylene oxide adduct, 38 parts by weight of ethylene glycol a...
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