Lithium secondary battery and electrodes for use therein
A technology of electrodes and ion batteries, applied in the field of rechargeable lithium secondary batteries
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[0049] LiFePO 4 (and its doped derivatives) have an olivine structure in the space group Pnma (No. 62) with set 1 (a=10.332 , b=6.010 , c=4.694 ). Obtain LiFePO from Süd-Chemie AG, Germany 4 particles. One sample consisted primarily of powder particles of mostly irregular shape (sample 232) and the other sample (sample 219) consisted of platelet-like particles.
[0050] In the present invention, the intensity ratio of two selected perpendicular peaks is determined by the selection of the signal assigned to the (020) crystal plane, which is the (301) plane. It is found that the (020) crystal plane always overlaps with the (211) plane, so the (211) plane is also considered when calculating the intensity ratio of the (020) plane.
[0051] X-ray diffraction (XRD) measurements were done on a Philips X'pert PW 3050 instrument with CuKα radiation (30 kV, 30 mA) acquired by graphite monochromator and variable slit.
[0052] When measuring electrode foils (substrate + particl...
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