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Method for measuring coating adhesive strength on a coating body using flexible material as substrate

A technology of adhesion strength and flexible materials, applied in the direction of measuring devices, analysis materials, instruments, etc., can solve the problems of low accuracy, achieve the effect of simple operation, overcome subjectivity, and optimize process parameters

Active Publication Date: 2010-10-13
SHANGHAI BYD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The purpose of the present invention is to overcome the shortcomings of the low accuracy of the existing method for measuring the strength of the pole piece dressing, and provide a method for measuring the adhesion strength of the coating on the coated body with a substrate of flexible materials.

Method used

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  • Method for measuring coating adhesive strength on a coating body using flexible material as substrate
  • Method for measuring coating adhesive strength on a coating body using flexible material as substrate
  • Method for measuring coating adhesive strength on a coating body using flexible material as substrate

Examples

Experimental program
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Embodiment approach

[0023] According to a specific embodiment of the present invention, the measuring method of coating adhesion strength provided by the present invention comprises the following steps:

[0024] (1) A surface with a coating at one end of the coated body is closely attached to the adhesive tape, and the coating is closely combined with the adhesive tape to the greatest extent by a pressure of 0.05-0.1 MPa;

[0025] (2) The coated body is bent 180° along the surface not bonded with the adhesive tape, so that the two ends of the coated body are parallel to each other;

[0026] (3) Fix the respective outer surfaces of the two ends parallel to each other on two rigid plates;

[0027] (4) Fix the two rigid boards on the two clamping ends of the peel force tester respectively, wherein the end with the adhesive tape is clamped and fixed by the clamping end which is the fixed end, and the unbonded end is clamped and fixed. The other end of the belt is held by the gripping end which is th...

preparation Embodiment 1

[0033] Preparation Example 1 A negative electrode sheet for measuring the dressing strength was prepared.

[0034] 100 parts by weight of negative electrode active material natural graphite, 1.0 parts by weight of binder polyvinylidene fluoride (PVDF) and 1.0 parts by weight of conductive agent carbon black are added in 120 parts by weight of N-methylpyrrolidone (NMP), then vacuum Stir in a mixer to form a stable and uniform negative electrode slurry. The slurry is evenly coated on a copper foil with a width of 400 mm and a thickness of 0.018 mm, and after drying at 120 ° C and rolling, it is cut on a slitting machine to obtain a size of 140.0 mm (length) × 45.0 mm ( width) × 0.145 mm (thickness) negative pole piece b1.

preparation Embodiment 2-5

[0036] Preparation Examples 2-5 Negative electrode sheets for measuring dressing strength were prepared.

[0037] According to the same method as Preparation Example 1, the size of the negative electrode sheet is 140.0 mm (length) × 45.0 mm (width) × 0.145 mm (thick), the difference is that the weight ratio of natural graphite to polyvinylidene fluoride 100: 1.5; 100: 2.0; 100: 2.5 and 100: 3.0, respectively, to obtain negative pole pieces b2-b5.

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Abstract

A coating adhesion strength measuring method for a coating body with substrate of flexible material comprises the following steps: acquiring the stripping force of the coating and calculating the adhesion strength according to the following formula: sigma 180 degrees=F / H, wherein, sigma 180 degrees representing the adhesion strength of the coating, F representing the stripping force of the coating, and H representing the width of a stripped coating under the action of the stripping force; the stripping force relating to the minimum tensile force needed for separating the coating and the substrate, and being obtained through the following steps: closely attaching and fixing one end of the coating body with coating surface and an adhesive strip with an adhesion strength being not less than the adhesion strength required by the coating body, then bending part of the coating body which never sticks to the adhesive strip to 180 DEG, thereby enabling the two ends of the coating body to be in parallel and the two ends of part of the coating body never sticking to the adhesive strip to approach each other, and after that applying a tensile force to the other end of the coating along the extending direction of the other end of the coating body to separate the coating and the substrate. The method provided by the invention enables a user to know the adhesion strength of the coating on the coating body accurately and objectively with good repeatability and simple operation.

Description

technical field [0001] The invention relates to a method for measuring the adhesion strength of a coating on a coated body, in particular to a method for measuring the adhesion strength of a coating on a coated body whose substrate is a flexible material. Background technique [0002] The lithium-ion battery mainly includes a pole core and a non-aqueous electrolyte, the pole core and the non-aqueous electrolyte are sealed in the battery case, the pole core includes a battery electrode and a diaphragm, and the battery electrode includes a positive pole piece and a negative pole piece , the positive electrode sheet includes a positive electrode collector and a positive electrode material coated and / or filled on the positive electrode collector, and the negative electrode sheet includes a negative electrode collector and a negative electrode material coated and / or filled on the negative electrode collector . [0003] At present, most lithium battery manufacturers or scientific...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N19/04
Inventor 刁家喜高艺
Owner SHANGHAI BYD