Method for preparing high-performance conductive fiber

A conductive fiber, high-performance technology, applied in liquid chemical plating, metal material coating process, coating and other directions, can solve the problems of non-fiber metal plating method, large power resources, unfavorable popularization, etc., to achieve good electrical conductivity, Less energy consumption and less pollution

Inactive Publication Date: 2008-07-09
江苏奈特纳米科技有限公司
View PDF0 Cites 25 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

1) Traditional electroplating method: this method needs to consume a lot of power resources, and cyanide-containing electroplating is very polluting to the environment; 2, cyanide-free electroplating method: the deep plating ability and throwing ability of this method need to be improved; 3) Vacuum sputtering coating m

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0058] In this embodiment, nylon is used as the matrix fiber

[0059] The first step is pretreatment. Soak the fibers with a solution of commercially available white cat detergent and absolute ethanol at a ratio of 1:5 (mass / volume). The soaking time is generally 10 to 20 minutes, depending on the cleanliness of the fibers. Depends on to remove surface stains and other impurities.

[0060] In the second step, roughening, the fiber is soaked in 1,2-dichloroethane for 20 minutes, and its surface is treated to increase its surface area and roughen its structure.

[0061] The third step, sensitization, is to soak the fiber with 2.5g / L tin dichloride solution for 15 minutes, so that a very thin metal catalytic layer is formed on the surface.

[0062] The fourth step, activation, soaks the fiber with 0.02g / L palladium chloride solution for 20 minutes.

[0063] The fifth step, electroless copper plating

[0064] Copper sulfate, disodium edetate, potassium sodium tartrate, sodium h...

Embodiment 2

[0085] In this embodiment, nylon is used as the matrix fiber

[0086] The first step, pretreatment, is to soak the fiber with 2g / L sodium hydroxide solution, usually for 15 minutes, to remove surface stains and other impurities.

[0087] In the second step, roughening, the fibers are surface treated by soaking them in xylene for 15 minutes to increase their surface area and roughen their structure.

[0088] The third step, sensitization, is to soak the fiber with 2g / L tin dichloride solution for 20 minutes, so that a very thin metal catalytic layer is formed on the surface.

[0089] The fourth step is activation. The fiber is soaked in 0.02g / L palladium chloride solution for 20 minutes, so that the palladium colloid replaces tin ions to form a metal catalytic layer.

[0090] The fifth step, electroless copper plating

[0091] Copper sulfate, disodium edetate, potassium sodium tartrate, sodium hydroxide and deionized water are prepared into an aqueous solution, and formaldehy...

Embodiment 3

[0112] In this embodiment, polyester is used as the base fiber

[0113] The first step is pretreatment. Soak the fiber with a solution of commercially available white cat detergent and absolute ethanol at a ratio of 1:4 (mass / volume). The soaking time is generally 10 to 20 minutes, depending on the cleanliness of the fiber. Depends on to remove surface stains and other impurities.

[0114] In the second step, roughening, the fiber is soaked in 1,2-dichloroethane for 20 minutes, and its surface is treated to increase its surface area and roughen its structure.

[0115] The third step, sensitization, is to soak the fiber with 2g / L tin dichloride solution for 20 minutes, so that a very thin metal catalytic layer is formed on the surface.

[0116] In the fourth step, activation, the fiber is soaked in 0.02 g / L palladium chloride solution for 20 minutes to obtain a palladium-coated metal catalyst layer.

[0117] The fifth step, electroless copper plating

[0118] Copper sulfate,...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The invention relates to a method for preparing a high performance conductive fiber, which comprises the following steps: V1ing, pretreatment and washing. V2ing, fiber is socked by coarsening agent to improve the surface structure of the fiber. V3ing, the fiber is socked by stannous chloride or cadmium chloride solution, and a layer of tin ions or cadmium ions are adsorbed on the surface of the fiber. V4ing, the fiber is socked by palladium chloride solution, and the tin ions or cadmium ions which are replaced by palladium colloid are adsorbed on the surface of the fiber. V5ing, electroless copper plating. V6ing, after being socked by oxalic acid solution, the fiber is dried. V7ing, the fiber which is plated with copper is socked and treated by tin dichloride solution. V8ing, the copper-plating fiber is socked by palladium chloride solution, and the tin ions or cadmium ions which are replaced by palladium colloid are adsorbed on the surface of the fiber. V9ing, chemical nickel plating. V10ing, after being socked by deionized water, the fiber is dried, and a product is obtained. The invention has small pollution to environment and less energy dissipation, and is easy to industrially produce. The conductive fiber which is prepared using the invention has excellent conductivity, the resistance of the specific surface area is 1-10 ohm, the original characteristics of the fiber is preserved, and the high performance conductive fiber is capable of being used for various non-woven fabrics.

Description

technical field [0001] The invention provides a preparation method of high-performance conductive fiber. In the method, a metal conductive thin layer is plated on the surface of ordinary fiber so that the fiber has antistatic and radiation-proof functions. Background technique [0002] With the continuous improvement of social productivity and the rapid development of science and technology, the process of urban modernization and industrialization is also getting faster and faster, and the resulting environmental pollution problems are becoming increasingly prominent. The arrival of the era of electrical appliances has gradually caused electromagnetic radiation pollution. Become another source of pollution after water pollution, air pollution and noise pollution. Crisis and opportunity coexist. After the popularization of electronic products, various anti-electromagnetic shielding products are born accordingly. As the clothes that are most closely related to people's daily ...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
IPC IPC(8): C23C18/16C23C18/18C23C18/22C23C18/28C23C18/30C23C18/40
Inventor 宋伟韩克让陈宝生
Owner 江苏奈特纳米科技有限公司
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap